4-(4-Chloro­phen­yl)-1-(2-hydr­oxy-2,2-di­phenyl­acet­yl)thio­semicarbazide

The asymmetric unit of the title compound, C(21)H(18)ClN(3)O(2)S, contains two mol­ecules in which the bond lengths and angles are almost identical. Intra­molecular N—H⋯S hydrogen bonds result in the formation of two five-membered rings. In the crystal structure, inter­molecular N—H⋯O hydrogen bonds...

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Detalles Bibliográficos
Autores principales: Abu-Safieh, Kayed A., Khanfar, Monther A., Eichele, Klaus, Ali, Basem Fares
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2008
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2959801/
https://www.ncbi.nlm.nih.gov/pubmed/21581282
http://dx.doi.org/10.1107/S1600536808035964
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author Abu-Safieh, Kayed A.
Khanfar, Monther A.
Eichele, Klaus
Ali, Basem Fares
author_facet Abu-Safieh, Kayed A.
Khanfar, Monther A.
Eichele, Klaus
Ali, Basem Fares
author_sort Abu-Safieh, Kayed A.
collection PubMed
description The asymmetric unit of the title compound, C(21)H(18)ClN(3)O(2)S, contains two mol­ecules in which the bond lengths and angles are almost identical. Intra­molecular N—H⋯S hydrogen bonds result in the formation of two five-membered rings. In the crystal structure, inter­molecular N—H⋯O hydrogen bonds link the mol­ecules into centrosymmetric dimers; these dimers are linked via inter­molecular O—H⋯S hydrogen bonds, leading to infinite corrugated layers parallel to the bc plane through R (2) (2)(16) ring motifs.
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spelling pubmed-29598012010-12-30 4-(4-Chloro­phen­yl)-1-(2-hydr­oxy-2,2-di­phenyl­acet­yl)thio­semicarbazide Abu-Safieh, Kayed A. Khanfar, Monther A. Eichele, Klaus Ali, Basem Fares Acta Crystallogr Sect E Struct Rep Online Organic Papers The asymmetric unit of the title compound, C(21)H(18)ClN(3)O(2)S, contains two mol­ecules in which the bond lengths and angles are almost identical. Intra­molecular N—H⋯S hydrogen bonds result in the formation of two five-membered rings. In the crystal structure, inter­molecular N—H⋯O hydrogen bonds link the mol­ecules into centrosymmetric dimers; these dimers are linked via inter­molecular O—H⋯S hydrogen bonds, leading to infinite corrugated layers parallel to the bc plane through R (2) (2)(16) ring motifs. International Union of Crystallography 2008-11-13 /pmc/articles/PMC2959801/ /pubmed/21581282 http://dx.doi.org/10.1107/S1600536808035964 Text en © Abu-Safieh et al. 2008 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Abu-Safieh, Kayed A.
Khanfar, Monther A.
Eichele, Klaus
Ali, Basem Fares
4-(4-Chloro­phen­yl)-1-(2-hydr­oxy-2,2-di­phenyl­acet­yl)thio­semicarbazide
title 4-(4-Chloro­phen­yl)-1-(2-hydr­oxy-2,2-di­phenyl­acet­yl)thio­semicarbazide
title_full 4-(4-Chloro­phen­yl)-1-(2-hydr­oxy-2,2-di­phenyl­acet­yl)thio­semicarbazide
title_fullStr 4-(4-Chloro­phen­yl)-1-(2-hydr­oxy-2,2-di­phenyl­acet­yl)thio­semicarbazide
title_full_unstemmed 4-(4-Chloro­phen­yl)-1-(2-hydr­oxy-2,2-di­phenyl­acet­yl)thio­semicarbazide
title_short 4-(4-Chloro­phen­yl)-1-(2-hydr­oxy-2,2-di­phenyl­acet­yl)thio­semicarbazide
title_sort 4-(4-chloro­phen­yl)-1-(2-hydr­oxy-2,2-di­phenyl­acet­yl)thio­semicarbazide
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2959801/
https://www.ncbi.nlm.nih.gov/pubmed/21581282
http://dx.doi.org/10.1107/S1600536808035964
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AT eicheleklaus 44chlorophenyl12hydroxy22diphenylacetylthiosemicarbazide
AT alibasemfares 44chlorophenyl12hydroxy22diphenylacetylthiosemicarbazide

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