N-[4-Chloro-2-methyl-6-(N-methyl­car­bam­oyl)phen­yl]-1-(3-chloro-2-pyrid­yl)-3-trifluoro­meth­yl-1H-pyrazole-5-carboxamide

In the title compound, C(19)H(14)Cl(2)F(3)N(5)O(2), which shows insecticidal activity, the dihedral angle between the pyrazole and pyridine rings is 68.15 (16)°. In the crystal structure, the mol­ecules are linked by N—H⋯O and C—H⋯O hydrogen bonds and an intra­molecular N—H⋯O inter­action also occur...

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Detalles Bibliográficos
Autores principales: Yang, Huibin, Yu, Haibo, Li, Bin
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2008
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2959817/
https://www.ncbi.nlm.nih.gov/pubmed/21581350
http://dx.doi.org/10.1107/S1600536808037604
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author Yang, Huibin
Yu, Haibo
Li, Bin
author_facet Yang, Huibin
Yu, Haibo
Li, Bin
author_sort Yang, Huibin
collection PubMed
description In the title compound, C(19)H(14)Cl(2)F(3)N(5)O(2), which shows insecticidal activity, the dihedral angle between the pyrazole and pyridine rings is 68.15 (16)°. In the crystal structure, the mol­ecules are linked by N—H⋯O and C—H⋯O hydrogen bonds and an intra­molecular N—H⋯O inter­action also occurs. The F atoms of the –CF(3) group are disordered over two sets of sites in a 0.800 (8):0.200 (8) ratio.
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spelling pubmed-29598172010-12-30 N-[4-Chloro-2-methyl-6-(N-methyl­car­bam­oyl)phen­yl]-1-(3-chloro-2-pyrid­yl)-3-trifluoro­meth­yl-1H-pyrazole-5-carboxamide Yang, Huibin Yu, Haibo Li, Bin Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(19)H(14)Cl(2)F(3)N(5)O(2), which shows insecticidal activity, the dihedral angle between the pyrazole and pyridine rings is 68.15 (16)°. In the crystal structure, the mol­ecules are linked by N—H⋯O and C—H⋯O hydrogen bonds and an intra­molecular N—H⋯O inter­action also occurs. The F atoms of the –CF(3) group are disordered over two sets of sites in a 0.800 (8):0.200 (8) ratio. International Union of Crystallography 2008-11-20 /pmc/articles/PMC2959817/ /pubmed/21581350 http://dx.doi.org/10.1107/S1600536808037604 Text en © Yang et al. 2008 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Yang, Huibin
Yu, Haibo
Li, Bin
N-[4-Chloro-2-methyl-6-(N-methyl­car­bam­oyl)phen­yl]-1-(3-chloro-2-pyrid­yl)-3-trifluoro­meth­yl-1H-pyrazole-5-carboxamide
title N-[4-Chloro-2-methyl-6-(N-methyl­car­bam­oyl)phen­yl]-1-(3-chloro-2-pyrid­yl)-3-trifluoro­meth­yl-1H-pyrazole-5-carboxamide
title_full N-[4-Chloro-2-methyl-6-(N-methyl­car­bam­oyl)phen­yl]-1-(3-chloro-2-pyrid­yl)-3-trifluoro­meth­yl-1H-pyrazole-5-carboxamide
title_fullStr N-[4-Chloro-2-methyl-6-(N-methyl­car­bam­oyl)phen­yl]-1-(3-chloro-2-pyrid­yl)-3-trifluoro­meth­yl-1H-pyrazole-5-carboxamide
title_full_unstemmed N-[4-Chloro-2-methyl-6-(N-methyl­car­bam­oyl)phen­yl]-1-(3-chloro-2-pyrid­yl)-3-trifluoro­meth­yl-1H-pyrazole-5-carboxamide
title_short N-[4-Chloro-2-methyl-6-(N-methyl­car­bam­oyl)phen­yl]-1-(3-chloro-2-pyrid­yl)-3-trifluoro­meth­yl-1H-pyrazole-5-carboxamide
title_sort n-[4-chloro-2-methyl-6-(n-methyl­car­bam­oyl)phen­yl]-1-(3-chloro-2-pyrid­yl)-3-trifluoro­meth­yl-1h-pyrazole-5-carboxamide
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2959817/
https://www.ncbi.nlm.nih.gov/pubmed/21581350
http://dx.doi.org/10.1107/S1600536808037604
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AT yuhaibo n4chloro2methyl6nmethylcarbamoylphenyl13chloro2pyridyl3trifluoromethyl1hpyrazole5carboxamide
AT libin n4chloro2methyl6nmethylcarbamoylphenyl13chloro2pyridyl3trifluoromethyl1hpyrazole5carboxamide

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