2,3-Difluoro-N-(2-pyrid­yl)benzamide

The title compound, C(12)H(8)F(2)N(2)O, crystallizes with two independent mol­ecules in the asymmetric unit. The independent mol­ecules differ slightly in conformation; the dihedral angles between the benzene and pyridine rings are 51.58 (5) and 49.97 (4)°. In the crystal structure, mol­ecules aggre...

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Detalles Bibliográficos
Autores principales: Gallagher, John F., McMahon, Joyce, Anderson, Frankie P., Lough, Alan J.
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2008
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2959868/
https://www.ncbi.nlm.nih.gov/pubmed/21581364
http://dx.doi.org/10.1107/S1600536808038269
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author Gallagher, John F.
McMahon, Joyce
Anderson, Frankie P.
Lough, Alan J.
author_facet Gallagher, John F.
McMahon, Joyce
Anderson, Frankie P.
Lough, Alan J.
author_sort Gallagher, John F.
collection PubMed
description The title compound, C(12)H(8)F(2)N(2)O, crystallizes with two independent mol­ecules in the asymmetric unit. The independent mol­ecules differ slightly in conformation; the dihedral angles between the benzene and pyridine rings are 51.58 (5) and 49.97 (4)°. In the crystal structure, mol­ecules aggregate via N—H⋯N(pyridine) inter­actions as hydrogen-bonded dimers with the structural motif R (2) (2)(8), and these dimers are linked via C—H⋯O inter­actions to form a supra­molecular chain.
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spelling pubmed-29598682010-12-30 2,3-Difluoro-N-(2-pyrid­yl)benzamide Gallagher, John F. McMahon, Joyce Anderson, Frankie P. Lough, Alan J. Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(12)H(8)F(2)N(2)O, crystallizes with two independent mol­ecules in the asymmetric unit. The independent mol­ecules differ slightly in conformation; the dihedral angles between the benzene and pyridine rings are 51.58 (5) and 49.97 (4)°. In the crystal structure, mol­ecules aggregate via N—H⋯N(pyridine) inter­actions as hydrogen-bonded dimers with the structural motif R (2) (2)(8), and these dimers are linked via C—H⋯O inter­actions to form a supra­molecular chain. International Union of Crystallography 2008-11-20 /pmc/articles/PMC2959868/ /pubmed/21581364 http://dx.doi.org/10.1107/S1600536808038269 Text en © Gallagher et al. 2008 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Gallagher, John F.
McMahon, Joyce
Anderson, Frankie P.
Lough, Alan J.
2,3-Difluoro-N-(2-pyrid­yl)benzamide
title 2,3-Difluoro-N-(2-pyrid­yl)benzamide
title_full 2,3-Difluoro-N-(2-pyrid­yl)benzamide
title_fullStr 2,3-Difluoro-N-(2-pyrid­yl)benzamide
title_full_unstemmed 2,3-Difluoro-N-(2-pyrid­yl)benzamide
title_short 2,3-Difluoro-N-(2-pyrid­yl)benzamide
title_sort 2,3-difluoro-n-(2-pyrid­yl)benzamide
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2959868/
https://www.ncbi.nlm.nih.gov/pubmed/21581364
http://dx.doi.org/10.1107/S1600536808038269
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AT mcmahonjoyce 23difluoron2pyridylbenzamide
AT andersonfrankiep 23difluoron2pyridylbenzamide
AT loughalanj 23difluoron2pyridylbenzamide

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