(4R)-4-(2-Allyl-2H-1,2,3-triazol-4-yl)-1,2-O-isopropyl­idene-l-threose

X-ray crystallography unequivocally confirmed the structure of the title compound, C(12)H(17)N(3)O(4), as (4R)-4-(2-allyl-2H-1,2,3-triazol-4-yl)-1,2-O-isopropyl­idene-l-threose. The absolute configuration was determined by the use of d-glucorono-3,6-lactone as the starting material. The crystal stru...

Descripción completa

Detalles Bibliográficos
Autores principales: Jenkinson, Sarah F., Best, Daniel, Wilson, Francis X., Fleet, George W. J., Watkin, David J.
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2008
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2959937/
https://www.ncbi.nlm.nih.gov/pubmed/21581334
http://dx.doi.org/10.1107/S1600536808036416
_version_ 1782188619263377408
author Jenkinson, Sarah F.
Best, Daniel
Wilson, Francis X.
Fleet, George W. J.
Watkin, David J.
author_facet Jenkinson, Sarah F.
Best, Daniel
Wilson, Francis X.
Fleet, George W. J.
Watkin, David J.
author_sort Jenkinson, Sarah F.
collection PubMed
description X-ray crystallography unequivocally confirmed the structure of the title compound, C(12)H(17)N(3)O(4), as (4R)-4-(2-allyl-2H-1,2,3-triazol-4-yl)-1,2-O-isopropyl­idene-l-threose. The absolute configuration was determined by the use of d-glucorono-3,6-lactone as the starting material. The crystal structure consists of hydrogen-bonded chains of mol­ecules running parallel to the a axis. There are no unusual packing features.
format Text
id pubmed-2959937
institution National Center for Biotechnology Information
language English
publishDate 2008
publisher International Union of Crystallography
record_format MEDLINE/PubMed
spelling pubmed-29599372010-12-30 (4R)-4-(2-Allyl-2H-1,2,3-triazol-4-yl)-1,2-O-isopropyl­idene-l-threose Jenkinson, Sarah F. Best, Daniel Wilson, Francis X. Fleet, George W. J. Watkin, David J. Acta Crystallogr Sect E Struct Rep Online Organic Papers X-ray crystallography unequivocally confirmed the structure of the title compound, C(12)H(17)N(3)O(4), as (4R)-4-(2-allyl-2H-1,2,3-triazol-4-yl)-1,2-O-isopropyl­idene-l-threose. The absolute configuration was determined by the use of d-glucorono-3,6-lactone as the starting material. The crystal structure consists of hydrogen-bonded chains of mol­ecules running parallel to the a axis. There are no unusual packing features. International Union of Crystallography 2008-11-13 /pmc/articles/PMC2959937/ /pubmed/21581334 http://dx.doi.org/10.1107/S1600536808036416 Text en © Jenkinson et al. 2008 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Jenkinson, Sarah F.
Best, Daniel
Wilson, Francis X.
Fleet, George W. J.
Watkin, David J.
(4R)-4-(2-Allyl-2H-1,2,3-triazol-4-yl)-1,2-O-isopropyl­idene-l-threose
title (4R)-4-(2-Allyl-2H-1,2,3-triazol-4-yl)-1,2-O-isopropyl­idene-l-threose
title_full (4R)-4-(2-Allyl-2H-1,2,3-triazol-4-yl)-1,2-O-isopropyl­idene-l-threose
title_fullStr (4R)-4-(2-Allyl-2H-1,2,3-triazol-4-yl)-1,2-O-isopropyl­idene-l-threose
title_full_unstemmed (4R)-4-(2-Allyl-2H-1,2,3-triazol-4-yl)-1,2-O-isopropyl­idene-l-threose
title_short (4R)-4-(2-Allyl-2H-1,2,3-triazol-4-yl)-1,2-O-isopropyl­idene-l-threose
title_sort (4r)-4-(2-allyl-2h-1,2,3-triazol-4-yl)-1,2-o-isopropyl­idene-l-threose
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2959937/
https://www.ncbi.nlm.nih.gov/pubmed/21581334
http://dx.doi.org/10.1107/S1600536808036416
work_keys_str_mv AT jenkinsonsarahf 4r42allyl2h123triazol4yl12oisopropylidenelthreose
AT bestdaniel 4r42allyl2h123triazol4yl12oisopropylidenelthreose
AT wilsonfrancisx 4r42allyl2h123triazol4yl12oisopropylidenelthreose
AT fleetgeorgewj 4r42allyl2h123triazol4yl12oisopropylidenelthreose
AT watkindavidj 4r42allyl2h123triazol4yl12oisopropylidenelthreose

Ejemplares similares