Bis{4-[(3-phenyl­allyl­idene)amino]cyclo­hexyl}methane trichloro­methane solvate

The title compound, C(31)H(38)N(2), was prepared from bis­(4-amino­cyclo­hexyl)methane and two equivalents of cinnamaldehyde. The cyclo­hexyl groups each show a chair conformation and the α,β-unsaturated imine side chains are all-trans configured. Two mol­ecules of the title compound as well as two...

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Detalles Bibliográficos
Autores principales: Menzel, Roberto, Göbel, Angela, Görls, Helmar, Imhof, Wolfgang
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2008
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2959948/
https://www.ncbi.nlm.nih.gov/pubmed/21581335
http://dx.doi.org/10.1107/S1600536808037380
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author Menzel, Roberto
Göbel, Angela
Görls, Helmar
Imhof, Wolfgang
author_facet Menzel, Roberto
Göbel, Angela
Görls, Helmar
Imhof, Wolfgang
author_sort Menzel, Roberto
collection PubMed
description The title compound, C(31)H(38)N(2), was prepared from bis­(4-amino­cyclo­hexyl)methane and two equivalents of cinnamaldehyde. The cyclo­hexyl groups each show a chair conformation and the α,β-unsaturated imine side chains are all-trans configured. Two mol­ecules of the title compound as well as two trichloromethane solvent mol­ecules are present in the asymmetric unit. The solvent mol­ecules inter­act with the diimines via weak C—H⋯N hydrogen bonds.
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spelling pubmed-29599482010-12-30 Bis{4-[(3-phenyl­allyl­idene)amino]cyclo­hexyl}methane trichloro­methane solvate Menzel, Roberto Göbel, Angela Görls, Helmar Imhof, Wolfgang Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(31)H(38)N(2), was prepared from bis­(4-amino­cyclo­hexyl)methane and two equivalents of cinnamaldehyde. The cyclo­hexyl groups each show a chair conformation and the α,β-unsaturated imine side chains are all-trans configured. Two mol­ecules of the title compound as well as two trichloromethane solvent mol­ecules are present in the asymmetric unit. The solvent mol­ecules inter­act with the diimines via weak C—H⋯N hydrogen bonds. International Union of Crystallography 2008-11-13 /pmc/articles/PMC2959948/ /pubmed/21581335 http://dx.doi.org/10.1107/S1600536808037380 Text en © Menzel et al. 2008 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Menzel, Roberto
Göbel, Angela
Görls, Helmar
Imhof, Wolfgang
Bis{4-[(3-phenyl­allyl­idene)amino]cyclo­hexyl}methane trichloro­methane solvate
title Bis{4-[(3-phenyl­allyl­idene)amino]cyclo­hexyl}methane trichloro­methane solvate
title_full Bis{4-[(3-phenyl­allyl­idene)amino]cyclo­hexyl}methane trichloro­methane solvate
title_fullStr Bis{4-[(3-phenyl­allyl­idene)amino]cyclo­hexyl}methane trichloro­methane solvate
title_full_unstemmed Bis{4-[(3-phenyl­allyl­idene)amino]cyclo­hexyl}methane trichloro­methane solvate
title_short Bis{4-[(3-phenyl­allyl­idene)amino]cyclo­hexyl}methane trichloro­methane solvate
title_sort bis{4-[(3-phenyl­allyl­idene)amino]cyclo­hexyl}methane trichloro­methane solvate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2959948/
https://www.ncbi.nlm.nih.gov/pubmed/21581335
http://dx.doi.org/10.1107/S1600536808037380
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AT gorlshelmar bis43phenylallylideneaminocyclohexylmethanetrichloromethanesolvate
AT imhofwolfgang bis43phenylallylideneaminocyclohexylmethanetrichloromethanesolvate

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