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2-(4-Chloro­phen­yl)-5-{3,4-dibut­oxy-5-[5-(4-chloro­phen­yl)-1,3,4-oxadiazol-2-yl]thio­phen-2-yl}-1,3,4-oxadiazole

In the title compound, C(28)H(26)Cl(2)N(4)O(4)S, the dihedral angles between the two chloro­phenyl rings and the two oxadiazol rings are 10.51 (4)° and 13.55 (3)°, respectively. The thio­phene ring is oriented at dihedral angles of 5.59 (4)°, 8.33 (4)° and 4.41 (4)°, 11.05 (3)°, respectively, with r...

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Detalles Bibliográficos
Autores principales: Li, Hai-Lin, Wang, Hong-Wei, Lu, Ran-Zhe, Wang, Hai-Bo
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2008
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2959962/
https://www.ncbi.nlm.nih.gov/pubmed/21581276
http://dx.doi.org/10.1107/S1600536808035848
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author Li, Hai-Lin
Wang, Hong-Wei
Lu, Ran-Zhe
Wang, Hai-Bo
author_facet Li, Hai-Lin
Wang, Hong-Wei
Lu, Ran-Zhe
Wang, Hai-Bo
author_sort Li, Hai-Lin
collection PubMed
description In the title compound, C(28)H(26)Cl(2)N(4)O(4)S, the dihedral angles between the two chloro­phenyl rings and the two oxadiazol rings are 10.51 (4)° and 13.55 (3)°, respectively. The thio­phene ring is oriented at dihedral angles of 5.59 (4)°, 8.33 (4)° and 4.41 (4)°, 11.05 (3)°, respectively, with respect to the two oxadiazol and the two chloro­phenyl rings. The intra­molecular C—H⋯O hydrogen bond results in the formation of a five-membered ring. In the crystal structure, π–π contacts between the oxadiazol rings, the chloro­phenyl rings and the chloro­phenyl and oxadiazol rings [centroid–centroid distances = 3.428 (3) Å, 3.750 (3) Å and 3.768 (3) Å, respectively] are present.
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spelling pubmed-29599622010-12-30 2-(4-Chloro­phen­yl)-5-{3,4-dibut­oxy-5-[5-(4-chloro­phen­yl)-1,3,4-oxadiazol-2-yl]thio­phen-2-yl}-1,3,4-oxadiazole Li, Hai-Lin Wang, Hong-Wei Lu, Ran-Zhe Wang, Hai-Bo Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(28)H(26)Cl(2)N(4)O(4)S, the dihedral angles between the two chloro­phenyl rings and the two oxadiazol rings are 10.51 (4)° and 13.55 (3)°, respectively. The thio­phene ring is oriented at dihedral angles of 5.59 (4)°, 8.33 (4)° and 4.41 (4)°, 11.05 (3)°, respectively, with respect to the two oxadiazol and the two chloro­phenyl rings. The intra­molecular C—H⋯O hydrogen bond results in the formation of a five-membered ring. In the crystal structure, π–π contacts between the oxadiazol rings, the chloro­phenyl rings and the chloro­phenyl and oxadiazol rings [centroid–centroid distances = 3.428 (3) Å, 3.750 (3) Å and 3.768 (3) Å, respectively] are present. International Union of Crystallography 2008-11-08 /pmc/articles/PMC2959962/ /pubmed/21581276 http://dx.doi.org/10.1107/S1600536808035848 Text en © Li et al. 2008 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Li, Hai-Lin
Wang, Hong-Wei
Lu, Ran-Zhe
Wang, Hai-Bo
2-(4-Chloro­phen­yl)-5-{3,4-dibut­oxy-5-[5-(4-chloro­phen­yl)-1,3,4-oxadiazol-2-yl]thio­phen-2-yl}-1,3,4-oxadiazole
title 2-(4-Chloro­phen­yl)-5-{3,4-dibut­oxy-5-[5-(4-chloro­phen­yl)-1,3,4-oxadiazol-2-yl]thio­phen-2-yl}-1,3,4-oxadiazole
title_full 2-(4-Chloro­phen­yl)-5-{3,4-dibut­oxy-5-[5-(4-chloro­phen­yl)-1,3,4-oxadiazol-2-yl]thio­phen-2-yl}-1,3,4-oxadiazole
title_fullStr 2-(4-Chloro­phen­yl)-5-{3,4-dibut­oxy-5-[5-(4-chloro­phen­yl)-1,3,4-oxadiazol-2-yl]thio­phen-2-yl}-1,3,4-oxadiazole
title_full_unstemmed 2-(4-Chloro­phen­yl)-5-{3,4-dibut­oxy-5-[5-(4-chloro­phen­yl)-1,3,4-oxadiazol-2-yl]thio­phen-2-yl}-1,3,4-oxadiazole
title_short 2-(4-Chloro­phen­yl)-5-{3,4-dibut­oxy-5-[5-(4-chloro­phen­yl)-1,3,4-oxadiazol-2-yl]thio­phen-2-yl}-1,3,4-oxadiazole
title_sort 2-(4-chloro­phen­yl)-5-{3,4-dibut­oxy-5-[5-(4-chloro­phen­yl)-1,3,4-oxadiazol-2-yl]thio­phen-2-yl}-1,3,4-oxadiazole
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2959962/
https://www.ncbi.nlm.nih.gov/pubmed/21581276
http://dx.doi.org/10.1107/S1600536808035848
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