2,2′,4,4′,6,6′-Hexamethyl-N-(3-phthalimidoprop­yl)-N,N′-(propane-1,3-di­yl)dibenzene­sulfonamide

In the title compound, C(32)H(38)N(3)O(6)S(2), an inter­mediate in the synthesis of polyamine drugs, the dihedral angle between the phenyl rings of the two 2,4,6-trimethyl­benzene­sulfonyl groups is 27.1 (3)°. In the crystal structure, mol­ecules are linked by inter­molecular N—H⋯O hydrogen bonds, t...

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Detalles Bibliográficos
Autores principales: Wang, Yu-Xia, Cheng, Peng-Fei, Wang, Chao-Jie
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2008
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2960108/
https://www.ncbi.nlm.nih.gov/pubmed/21581267
http://dx.doi.org/10.1107/S1600536808036003
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author Wang, Yu-Xia
Cheng, Peng-Fei
Wang, Chao-Jie
author_facet Wang, Yu-Xia
Cheng, Peng-Fei
Wang, Chao-Jie
author_sort Wang, Yu-Xia
collection PubMed
description In the title compound, C(32)H(38)N(3)O(6)S(2), an inter­mediate in the synthesis of polyamine drugs, the dihedral angle between the phenyl rings of the two 2,4,6-trimethyl­benzene­sulfonyl groups is 27.1 (3)°. In the crystal structure, mol­ecules are linked by inter­molecular N—H⋯O hydrogen bonds, thereby forming an infinite one-dimensional chain propagating along [010].
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spelling pubmed-29601082010-12-30 2,2′,4,4′,6,6′-Hexamethyl-N-(3-phthalimidoprop­yl)-N,N′-(propane-1,3-di­yl)dibenzene­sulfonamide Wang, Yu-Xia Cheng, Peng-Fei Wang, Chao-Jie Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(32)H(38)N(3)O(6)S(2), an inter­mediate in the synthesis of polyamine drugs, the dihedral angle between the phenyl rings of the two 2,4,6-trimethyl­benzene­sulfonyl groups is 27.1 (3)°. In the crystal structure, mol­ecules are linked by inter­molecular N—H⋯O hydrogen bonds, thereby forming an infinite one-dimensional chain propagating along [010]. International Union of Crystallography 2008-11-08 /pmc/articles/PMC2960108/ /pubmed/21581267 http://dx.doi.org/10.1107/S1600536808036003 Text en © Wang et al. 2008 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Wang, Yu-Xia
Cheng, Peng-Fei
Wang, Chao-Jie
2,2′,4,4′,6,6′-Hexamethyl-N-(3-phthalimidoprop­yl)-N,N′-(propane-1,3-di­yl)dibenzene­sulfonamide
title 2,2′,4,4′,6,6′-Hexamethyl-N-(3-phthalimidoprop­yl)-N,N′-(propane-1,3-di­yl)dibenzene­sulfonamide
title_full 2,2′,4,4′,6,6′-Hexamethyl-N-(3-phthalimidoprop­yl)-N,N′-(propane-1,3-di­yl)dibenzene­sulfonamide
title_fullStr 2,2′,4,4′,6,6′-Hexamethyl-N-(3-phthalimidoprop­yl)-N,N′-(propane-1,3-di­yl)dibenzene­sulfonamide
title_full_unstemmed 2,2′,4,4′,6,6′-Hexamethyl-N-(3-phthalimidoprop­yl)-N,N′-(propane-1,3-di­yl)dibenzene­sulfonamide
title_short 2,2′,4,4′,6,6′-Hexamethyl-N-(3-phthalimidoprop­yl)-N,N′-(propane-1,3-di­yl)dibenzene­sulfonamide
title_sort 2,2′,4,4′,6,6′-hexamethyl-n-(3-phthalimidoprop­yl)-n,n′-(propane-1,3-di­yl)dibenzene­sulfonamide
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2960108/
https://www.ncbi.nlm.nih.gov/pubmed/21581267
http://dx.doi.org/10.1107/S1600536808036003
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