N,N′-Bis(4-methyl­phen­yl)naphthalene-1,4-dicarboxamide N,N-dimethyl­acetamide disolvate

The title compound, C(26)H(22)N(2)O(2)·2C(4)H(9)NO, crystallizes in an anti C=O orientation. The two amide groups are approximately perpendicular to the naphthalene ring system [dihedral angles = 88.89 (1) and 89.08 (1)°]. Each of the dimethyl­acetamide solvent mol­ecules are disordered over two pos...

Descripción completa

Detalles Bibliográficos
Autor principal: Jing, Lin-Hai
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2008
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2960113/
https://www.ncbi.nlm.nih.gov/pubmed/21581351
http://dx.doi.org/10.1107/S1600536808037422
_version_ 1782188661338537984
author Jing, Lin-Hai
author_facet Jing, Lin-Hai
author_sort Jing, Lin-Hai
collection PubMed
description The title compound, C(26)H(22)N(2)O(2)·2C(4)H(9)NO, crystallizes in an anti C=O orientation. The two amide groups are approximately perpendicular to the naphthalene ring system [dihedral angles = 88.89 (1) and 89.08 (1)°]. Each of the dimethyl­acetamide solvent mol­ecules are disordered over two positions, with occupancies of 0.655 (12):0.345 (12) and 0.531 (13):0.469 (13). The crystal packing is stabilized by N—H⋯O and C—H⋯O hydrogen bonds.
format Text
id pubmed-2960113
institution National Center for Biotechnology Information
language English
publishDate 2008
publisher International Union of Crystallography
record_format MEDLINE/PubMed
spelling pubmed-29601132010-12-30 N,N′-Bis(4-methyl­phen­yl)naphthalene-1,4-dicarboxamide N,N-dimethyl­acetamide disolvate Jing, Lin-Hai Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(26)H(22)N(2)O(2)·2C(4)H(9)NO, crystallizes in an anti C=O orientation. The two amide groups are approximately perpendicular to the naphthalene ring system [dihedral angles = 88.89 (1) and 89.08 (1)°]. Each of the dimethyl­acetamide solvent mol­ecules are disordered over two positions, with occupancies of 0.655 (12):0.345 (12) and 0.531 (13):0.469 (13). The crystal packing is stabilized by N—H⋯O and C—H⋯O hydrogen bonds. International Union of Crystallography 2008-11-20 /pmc/articles/PMC2960113/ /pubmed/21581351 http://dx.doi.org/10.1107/S1600536808037422 Text en © Lin-Hai Jing 2008 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Jing, Lin-Hai
N,N′-Bis(4-methyl­phen­yl)naphthalene-1,4-dicarboxamide N,N-dimethyl­acetamide disolvate
title N,N′-Bis(4-methyl­phen­yl)naphthalene-1,4-dicarboxamide N,N-dimethyl­acetamide disolvate
title_full N,N′-Bis(4-methyl­phen­yl)naphthalene-1,4-dicarboxamide N,N-dimethyl­acetamide disolvate
title_fullStr N,N′-Bis(4-methyl­phen­yl)naphthalene-1,4-dicarboxamide N,N-dimethyl­acetamide disolvate
title_full_unstemmed N,N′-Bis(4-methyl­phen­yl)naphthalene-1,4-dicarboxamide N,N-dimethyl­acetamide disolvate
title_short N,N′-Bis(4-methyl­phen­yl)naphthalene-1,4-dicarboxamide N,N-dimethyl­acetamide disolvate
title_sort n,n′-bis(4-methyl­phen­yl)naphthalene-1,4-dicarboxamide n,n-dimethyl­acetamide disolvate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2960113/
https://www.ncbi.nlm.nih.gov/pubmed/21581351
http://dx.doi.org/10.1107/S1600536808037422
work_keys_str_mv AT jinglinhai nnbis4methylphenylnaphthalene14dicarboxamidenndimethylacetamidedisolvate

Ejemplares similares