1,3-Di-4-pyridylpropane–4,4′-oxy­dibenzoic acid (1/1)

The hydro­thermal reaction of Cd(NO(3))(2)·4H(2)O, 1,3-di-4-pyridylpropane (BPP) and 4,4′-oxydibenzoic acid (OBA) led to the formation of the title compound, C(13)H(14)N(2)·C(14)H(10)O(5). The asymmetric unit consists of one mol­ecule of OBA and one of BPP. In the OBA mol­ecule, one COOH group is ne...

Descripción completa

Detalles Bibliográficos
Autores principales: Li, Guangzhe, Salim, Chris, Hinode, Hirofumi
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2008
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2960149/
https://www.ncbi.nlm.nih.gov/pubmed/21581232
http://dx.doi.org/10.1107/S160053680803331X
_version_ 1782188670009212928
author Li, Guangzhe
Salim, Chris
Hinode, Hirofumi
author_facet Li, Guangzhe
Salim, Chris
Hinode, Hirofumi
author_sort Li, Guangzhe
collection PubMed
description The hydro­thermal reaction of Cd(NO(3))(2)·4H(2)O, 1,3-di-4-pyridylpropane (BPP) and 4,4′-oxydibenzoic acid (OBA) led to the formation of the title compound, C(13)H(14)N(2)·C(14)H(10)O(5). The asymmetric unit consists of one mol­ecule of OBA and one of BPP. In the OBA mol­ecule, one COOH group is nearly planar with its attached benzene ring [dihedral angle = 0.9 (1)°], while the other COOH group is slightly twisted with a dihedral angle of 10.8 (3)°. The carboxyl groups form strong inter­molecular O—H⋯N hydrogen bonds with N atoms of the pyridine rings in BPP, linking the mol­ecules into zigzag chains.
format Text
id pubmed-2960149
institution National Center for Biotechnology Information
language English
publishDate 2008
publisher International Union of Crystallography
record_format MEDLINE/PubMed
spelling pubmed-29601492010-12-30 1,3-Di-4-pyridylpropane–4,4′-oxy­dibenzoic acid (1/1) Li, Guangzhe Salim, Chris Hinode, Hirofumi Acta Crystallogr Sect E Struct Rep Online Organic Papers The hydro­thermal reaction of Cd(NO(3))(2)·4H(2)O, 1,3-di-4-pyridylpropane (BPP) and 4,4′-oxydibenzoic acid (OBA) led to the formation of the title compound, C(13)H(14)N(2)·C(14)H(10)O(5). The asymmetric unit consists of one mol­ecule of OBA and one of BPP. In the OBA mol­ecule, one COOH group is nearly planar with its attached benzene ring [dihedral angle = 0.9 (1)°], while the other COOH group is slightly twisted with a dihedral angle of 10.8 (3)°. The carboxyl groups form strong inter­molecular O—H⋯N hydrogen bonds with N atoms of the pyridine rings in BPP, linking the mol­ecules into zigzag chains. International Union of Crystallography 2008-11-08 /pmc/articles/PMC2960149/ /pubmed/21581232 http://dx.doi.org/10.1107/S160053680803331X Text en © Li et al. 2008 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Li, Guangzhe
Salim, Chris
Hinode, Hirofumi
1,3-Di-4-pyridylpropane–4,4′-oxy­dibenzoic acid (1/1)
title 1,3-Di-4-pyridylpropane–4,4′-oxy­dibenzoic acid (1/1)
title_full 1,3-Di-4-pyridylpropane–4,4′-oxy­dibenzoic acid (1/1)
title_fullStr 1,3-Di-4-pyridylpropane–4,4′-oxy­dibenzoic acid (1/1)
title_full_unstemmed 1,3-Di-4-pyridylpropane–4,4′-oxy­dibenzoic acid (1/1)
title_short 1,3-Di-4-pyridylpropane–4,4′-oxy­dibenzoic acid (1/1)
title_sort 1,3-di-4-pyridylpropane–4,4′-oxy­dibenzoic acid (1/1)
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2960149/
https://www.ncbi.nlm.nih.gov/pubmed/21581232
http://dx.doi.org/10.1107/S160053680803331X
work_keys_str_mv AT liguangzhe 13di4pyridylpropane44oxydibenzoicacid11
AT salimchris 13di4pyridylpropane44oxydibenzoicacid11
AT hinodehirofumi 13di4pyridylpropane44oxydibenzoicacid11

Ejemplares similares