2-[Bis(5-chloro-2-pyridylamino)methyl]pyridine monohydrate

In the title compound, the dihedral angles between the 2-amino-5-chloro­pyridyl rings and the pyridine ring are 56.26 (6)° and 78.83 (5)°; the angle between the 2-amino-5-chloro­pyridyl rings is 72.42 (5)°. The solvent water mol­ecules are linked to the organic compound by N—H⋯O, O—H⋯O, N—H⋯N and O—...

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Detalles Bibliográficos
Autores principales: M. Boghaei, Davar, Najafpour, Mohammad Mahdi, McKee, Vickie
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2008
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2960150/
https://www.ncbi.nlm.nih.gov/pubmed/21581396
http://dx.doi.org/10.1107/S1600536808035940
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author M. Boghaei, Davar
Najafpour, Mohammad Mahdi
McKee, Vickie
author_facet M. Boghaei, Davar
Najafpour, Mohammad Mahdi
McKee, Vickie
author_sort M. Boghaei, Davar
collection PubMed
description In the title compound, the dihedral angles between the 2-amino-5-chloro­pyridyl rings and the pyridine ring are 56.26 (6)° and 78.83 (5)°; the angle between the 2-amino-5-chloro­pyridyl rings is 72.42 (5)°. The solvent water mol­ecules are linked to the organic compound by N—H⋯O, O—H⋯O, N—H⋯N and O—H⋯N hydrogen bonds. π⋯π Stacking inter­actions are also observed between the 2-amino-5-chloro­pyridyl rings (centroid⋯centroid distance = 3.243 Å).
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spelling pubmed-29601502010-12-30 2-[Bis(5-chloro-2-pyridylamino)methyl]pyridine monohydrate M. Boghaei, Davar Najafpour, Mohammad Mahdi McKee, Vickie Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, the dihedral angles between the 2-amino-5-chloro­pyridyl rings and the pyridine ring are 56.26 (6)° and 78.83 (5)°; the angle between the 2-amino-5-chloro­pyridyl rings is 72.42 (5)°. The solvent water mol­ecules are linked to the organic compound by N—H⋯O, O—H⋯O, N—H⋯N and O—H⋯N hydrogen bonds. π⋯π Stacking inter­actions are also observed between the 2-amino-5-chloro­pyridyl rings (centroid⋯centroid distance = 3.243 Å). International Union of Crystallography 2008-11-22 /pmc/articles/PMC2960150/ /pubmed/21581396 http://dx.doi.org/10.1107/S1600536808035940 Text en © M. Boghaei et al. 2008 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
M. Boghaei, Davar
Najafpour, Mohammad Mahdi
McKee, Vickie
2-[Bis(5-chloro-2-pyridylamino)methyl]pyridine monohydrate
title 2-[Bis(5-chloro-2-pyridylamino)methyl]pyridine monohydrate
title_full 2-[Bis(5-chloro-2-pyridylamino)methyl]pyridine monohydrate
title_fullStr 2-[Bis(5-chloro-2-pyridylamino)methyl]pyridine monohydrate
title_full_unstemmed 2-[Bis(5-chloro-2-pyridylamino)methyl]pyridine monohydrate
title_short 2-[Bis(5-chloro-2-pyridylamino)methyl]pyridine monohydrate
title_sort 2-[bis(5-chloro-2-pyridylamino)methyl]pyridine monohydrate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2960150/
https://www.ncbi.nlm.nih.gov/pubmed/21581396
http://dx.doi.org/10.1107/S1600536808035940
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AT najafpourmohammadmahdi 2bis5chloro2pyridylaminomethylpyridinemonohydrate
AT mckeevickie 2bis5chloro2pyridylaminomethylpyridinemonohydrate

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