4-(4-Bromo­phenyl­hydrazono)-1-(5-bromo­pyrimidin-2-yl)-3-methyl-2-pyrazolin-5-one

The asymmetric unit of the title compound, C(14)H(10)Br(2)N(6)O, contains two crystallographically independent mol­ecules. The pyrazole ring of one mol­ecule makes dihedral angles of 22.0 (3) and 3.5 (3)° with the pyrimidine and benzene rings, respectively; the corresponding values in the other mol­...

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Detalles Bibliográficos
Autores principales: Subramanyam, M., Lingappa, B., Thiruvalluvar, A., Butcher, R. J., Kalluraya, Balakrishna
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2008
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2960163/
https://www.ncbi.nlm.nih.gov/pubmed/21201394
http://dx.doi.org/10.1107/S1600536807067943
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author Subramanyam, M.
Lingappa, B.
Thiruvalluvar, A.
Butcher, R. J.
Kalluraya, Balakrishna
author_facet Subramanyam, M.
Lingappa, B.
Thiruvalluvar, A.
Butcher, R. J.
Kalluraya, Balakrishna
author_sort Subramanyam, M.
collection PubMed
description The asymmetric unit of the title compound, C(14)H(10)Br(2)N(6)O, contains two crystallographically independent mol­ecules. The pyrazole ring of one mol­ecule makes dihedral angles of 22.0 (3) and 3.5 (3)° with the pyrimidine and benzene rings, respectively; the corresponding values in the other mol­ecule are 9.2 (3) and 2.1 (3)°, respectively. The mol­ecules are linked by N—H⋯O, C—H⋯N and C—H⋯Br hydrogen bonds.
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spelling pubmed-29601632010-12-30 4-(4-Bromo­phenyl­hydrazono)-1-(5-bromo­pyrimidin-2-yl)-3-methyl-2-pyrazolin-5-one Subramanyam, M. Lingappa, B. Thiruvalluvar, A. Butcher, R. J. Kalluraya, Balakrishna Acta Crystallogr Sect E Struct Rep Online Organic Papers The asymmetric unit of the title compound, C(14)H(10)Br(2)N(6)O, contains two crystallographically independent mol­ecules. The pyrazole ring of one mol­ecule makes dihedral angles of 22.0 (3) and 3.5 (3)° with the pyrimidine and benzene rings, respectively; the corresponding values in the other mol­ecule are 9.2 (3) and 2.1 (3)°, respectively. The mol­ecules are linked by N—H⋯O, C—H⋯N and C—H⋯Br hydrogen bonds. International Union of Crystallography 2008-01-04 /pmc/articles/PMC2960163/ /pubmed/21201394 http://dx.doi.org/10.1107/S1600536807067943 Text en © International Union of Crystallography 2008 http://journals.iucr.org/services/termsofuse.html This is an open-access article distributed under the terms described at http://journals.iucr.org/services/termsofuse.html.
spellingShingle Organic Papers
Subramanyam, M.
Lingappa, B.
Thiruvalluvar, A.
Butcher, R. J.
Kalluraya, Balakrishna
4-(4-Bromo­phenyl­hydrazono)-1-(5-bromo­pyrimidin-2-yl)-3-methyl-2-pyrazolin-5-one
title 4-(4-Bromo­phenyl­hydrazono)-1-(5-bromo­pyrimidin-2-yl)-3-methyl-2-pyrazolin-5-one
title_full 4-(4-Bromo­phenyl­hydrazono)-1-(5-bromo­pyrimidin-2-yl)-3-methyl-2-pyrazolin-5-one
title_fullStr 4-(4-Bromo­phenyl­hydrazono)-1-(5-bromo­pyrimidin-2-yl)-3-methyl-2-pyrazolin-5-one
title_full_unstemmed 4-(4-Bromo­phenyl­hydrazono)-1-(5-bromo­pyrimidin-2-yl)-3-methyl-2-pyrazolin-5-one
title_short 4-(4-Bromo­phenyl­hydrazono)-1-(5-bromo­pyrimidin-2-yl)-3-methyl-2-pyrazolin-5-one
title_sort 4-(4-bromo­phenyl­hydrazono)-1-(5-bromo­pyrimidin-2-yl)-3-methyl-2-pyrazolin-5-one
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2960163/
https://www.ncbi.nlm.nih.gov/pubmed/21201394
http://dx.doi.org/10.1107/S1600536807067943
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