2-Anilino-3-benzoyl-4-(2,5-dichloro­phen­yl)-7,7-dimethyl-5-oxo-5,6,7,8-tetra­hydro-4H-benzo[b]pyran

The title compound, C(30)H(25)Cl(2)NO(3), was prepared by the reaction of 3-oxo-N,3-diphenyl­propane­thio­amide, 2,5-dichloro­benzaldehyde and 5,5-dimethyl-1,3-cyclo­hexa­nedione (1:1:1) in ethanol. The cyclohexene ring adopts a half-chair conformation. The crystal structure exhibits intra­molecular...

Descripción completa

Detalles Bibliográficos
Autores principales: Wen, Li-Rong, Sun, Ji-Hui, Ji, Chen, Xie, Huai-Yuan
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2008
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2960223/
https://www.ncbi.nlm.nih.gov/pubmed/21201435
http://dx.doi.org/10.1107/S1600536807068377
_version_ 1782188687700787200
author Wen, Li-Rong
Sun, Ji-Hui
Ji, Chen
Xie, Huai-Yuan
author_facet Wen, Li-Rong
Sun, Ji-Hui
Ji, Chen
Xie, Huai-Yuan
author_sort Wen, Li-Rong
collection PubMed
description The title compound, C(30)H(25)Cl(2)NO(3), was prepared by the reaction of 3-oxo-N,3-diphenyl­propane­thio­amide, 2,5-dichloro­benzaldehyde and 5,5-dimethyl-1,3-cyclo­hexa­nedione (1:1:1) in ethanol. The cyclohexene ring adopts a half-chair conformation. The crystal structure exhibits intra­molecular N—H⋯O and C—H⋯O, and inter­molecular C—H⋯O inter­actions.
format Text
id pubmed-2960223
institution National Center for Biotechnology Information
language English
publishDate 2008
publisher International Union of Crystallography
record_format MEDLINE/PubMed
spelling pubmed-29602232010-12-30 2-Anilino-3-benzoyl-4-(2,5-dichloro­phen­yl)-7,7-dimethyl-5-oxo-5,6,7,8-tetra­hydro-4H-benzo[b]pyran Wen, Li-Rong Sun, Ji-Hui Ji, Chen Xie, Huai-Yuan Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(30)H(25)Cl(2)NO(3), was prepared by the reaction of 3-oxo-N,3-diphenyl­propane­thio­amide, 2,5-dichloro­benzaldehyde and 5,5-dimethyl-1,3-cyclo­hexa­nedione (1:1:1) in ethanol. The cyclohexene ring adopts a half-chair conformation. The crystal structure exhibits intra­molecular N—H⋯O and C—H⋯O, and inter­molecular C—H⋯O inter­actions. International Union of Crystallography 2008-01-09 /pmc/articles/PMC2960223/ /pubmed/21201435 http://dx.doi.org/10.1107/S1600536807068377 Text en © International Union of Crystallography 2008 http://journals.iucr.org/services/termsofuse.html This is an open-access article distributed under the terms described at http://journals.iucr.org/services/termsofuse.html.
spellingShingle Organic Papers
Wen, Li-Rong
Sun, Ji-Hui
Ji, Chen
Xie, Huai-Yuan
2-Anilino-3-benzoyl-4-(2,5-dichloro­phen­yl)-7,7-dimethyl-5-oxo-5,6,7,8-tetra­hydro-4H-benzo[b]pyran
title 2-Anilino-3-benzoyl-4-(2,5-dichloro­phen­yl)-7,7-dimethyl-5-oxo-5,6,7,8-tetra­hydro-4H-benzo[b]pyran
title_full 2-Anilino-3-benzoyl-4-(2,5-dichloro­phen­yl)-7,7-dimethyl-5-oxo-5,6,7,8-tetra­hydro-4H-benzo[b]pyran
title_fullStr 2-Anilino-3-benzoyl-4-(2,5-dichloro­phen­yl)-7,7-dimethyl-5-oxo-5,6,7,8-tetra­hydro-4H-benzo[b]pyran
title_full_unstemmed 2-Anilino-3-benzoyl-4-(2,5-dichloro­phen­yl)-7,7-dimethyl-5-oxo-5,6,7,8-tetra­hydro-4H-benzo[b]pyran
title_short 2-Anilino-3-benzoyl-4-(2,5-dichloro­phen­yl)-7,7-dimethyl-5-oxo-5,6,7,8-tetra­hydro-4H-benzo[b]pyran
title_sort 2-anilino-3-benzoyl-4-(2,5-dichloro­phen­yl)-7,7-dimethyl-5-oxo-5,6,7,8-tetra­hydro-4h-benzo[b]pyran
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2960223/
https://www.ncbi.nlm.nih.gov/pubmed/21201435
http://dx.doi.org/10.1107/S1600536807068377
work_keys_str_mv AT wenlirong 2anilino3benzoyl425dichlorophenyl77dimethyl5oxo5678tetrahydro4hbenzobpyran
AT sunjihui 2anilino3benzoyl425dichlorophenyl77dimethyl5oxo5678tetrahydro4hbenzobpyran
AT jichen 2anilino3benzoyl425dichlorophenyl77dimethyl5oxo5678tetrahydro4hbenzobpyran
AT xiehuaiyuan 2anilino3benzoyl425dichlorophenyl77dimethyl5oxo5678tetrahydro4hbenzobpyran

Ejemplares similares