2-(4-Amino-5-thioxo-4,5-dihydro-1H-1,2,4-triazol-3-ylmeth­yl)isoindoline-1,3-dione

The title compound, C(11)H(9)N(5)O(2)S, was synthesized from N-phthaloylglycine and thio­carbohydrazide by the fusion method. This is the first report of a triazole derivative of N-phthaloylglycine. The title compound exists in the thione form. The mol­ecule is non-planar, with a dihedral angle betw...

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Detalles Bibliográficos
Autores principales: Yunus, Uzma, Tahir, Mohammad Kalim, Bhatti, Moazzam Hussain, Yousaf, Naveeda, Helliwell, Madeleine
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2008
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2960251/
https://www.ncbi.nlm.nih.gov/pubmed/21201502
http://dx.doi.org/10.1107/S1600536808001189
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author Yunus, Uzma
Tahir, Mohammad Kalim
Bhatti, Moazzam Hussain
Yousaf, Naveeda
Helliwell, Madeleine
author_facet Yunus, Uzma
Tahir, Mohammad Kalim
Bhatti, Moazzam Hussain
Yousaf, Naveeda
Helliwell, Madeleine
author_sort Yunus, Uzma
collection PubMed
description The title compound, C(11)H(9)N(5)O(2)S, was synthesized from N-phthaloylglycine and thio­carbohydrazide by the fusion method. This is the first report of a triazole derivative of N-phthaloylglycine. The title compound exists in the thione form. The mol­ecule is non-planar, with a dihedral angle between the isoindoline ring system and the triazole ring system of 82.24 (5)°. The crystal structure is stabilized by inter­molecular hydrogen bonding linking the mol­ecules into a three-dimensional network.
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spelling pubmed-29602512010-12-30 2-(4-Amino-5-thioxo-4,5-dihydro-1H-1,2,4-triazol-3-ylmeth­yl)isoindoline-1,3-dione Yunus, Uzma Tahir, Mohammad Kalim Bhatti, Moazzam Hussain Yousaf, Naveeda Helliwell, Madeleine Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(11)H(9)N(5)O(2)S, was synthesized from N-phthaloylglycine and thio­carbohydrazide by the fusion method. This is the first report of a triazole derivative of N-phthaloylglycine. The title compound exists in the thione form. The mol­ecule is non-planar, with a dihedral angle between the isoindoline ring system and the triazole ring system of 82.24 (5)°. The crystal structure is stabilized by inter­molecular hydrogen bonding linking the mol­ecules into a three-dimensional network. International Union of Crystallography 2008-01-23 /pmc/articles/PMC2960251/ /pubmed/21201502 http://dx.doi.org/10.1107/S1600536808001189 Text en © International Union of Crystallography 2008 http://journals.iucr.org/services/termsofuse.html This is an open-access article distributed under the terms described at http://journals.iucr.org/services/termsofuse.html.
spellingShingle Organic Papers
Yunus, Uzma
Tahir, Mohammad Kalim
Bhatti, Moazzam Hussain
Yousaf, Naveeda
Helliwell, Madeleine
2-(4-Amino-5-thioxo-4,5-dihydro-1H-1,2,4-triazol-3-ylmeth­yl)isoindoline-1,3-dione
title 2-(4-Amino-5-thioxo-4,5-dihydro-1H-1,2,4-triazol-3-ylmeth­yl)isoindoline-1,3-dione
title_full 2-(4-Amino-5-thioxo-4,5-dihydro-1H-1,2,4-triazol-3-ylmeth­yl)isoindoline-1,3-dione
title_fullStr 2-(4-Amino-5-thioxo-4,5-dihydro-1H-1,2,4-triazol-3-ylmeth­yl)isoindoline-1,3-dione
title_full_unstemmed 2-(4-Amino-5-thioxo-4,5-dihydro-1H-1,2,4-triazol-3-ylmeth­yl)isoindoline-1,3-dione
title_short 2-(4-Amino-5-thioxo-4,5-dihydro-1H-1,2,4-triazol-3-ylmeth­yl)isoindoline-1,3-dione
title_sort 2-(4-amino-5-thioxo-4,5-dihydro-1h-1,2,4-triazol-3-ylmeth­yl)isoindoline-1,3-dione
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2960251/
https://www.ncbi.nlm.nih.gov/pubmed/21201502
http://dx.doi.org/10.1107/S1600536808001189
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