Ethyl 7-amino-1-cyclo­propyl-6-fluoro-8-meth­oxy-4-oxo-1,4-dihydro­quinoline-3-carboxyl­ate monohydrate

In the title compound, C(16)H(17)FN(2)O(4)·H(2)O, the dihedral angle between the heterocyclic ring and the benzene ring is 5.77 (9)°, that between the heterocycle and the ethoxy­carbonyl plane is 15.5 (1)°, and that between the heterocyclic ring and the cyclopropane ring is 67.75 (13)°. In the cryst...

Descripción completa

Detalles Bibliográficos
Autores principales: Pan, Jia, Yang, Li, Mao, Zhi-Hua, Weng, Ling-Ling
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2008
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2960450/
https://www.ncbi.nlm.nih.gov/pubmed/21201546
http://dx.doi.org/10.1107/S1600536808002547
_version_ 1782188742544457728
author Pan, Jia
Yang, Li
Mao, Zhi-Hua
Weng, Ling-Ling
author_facet Pan, Jia
Yang, Li
Mao, Zhi-Hua
Weng, Ling-Ling
author_sort Pan, Jia
collection PubMed
description In the title compound, C(16)H(17)FN(2)O(4)·H(2)O, the dihedral angle between the heterocyclic ring and the benzene ring is 5.77 (9)°, that between the heterocycle and the ethoxy­carbonyl plane is 15.5 (1)°, and that between the heterocyclic ring and the cyclopropane ring is 67.75 (13)°. In the crystal structure, mol­ecules are linked into a ribbon-like structure along the c axis by N—H⋯O and O—H⋯O hydrogen bonds.
format Text
id pubmed-2960450
institution National Center for Biotechnology Information
language English
publishDate 2008
publisher International Union of Crystallography
record_format MEDLINE/PubMed
spelling pubmed-29604502010-12-30 Ethyl 7-amino-1-cyclo­propyl-6-fluoro-8-meth­oxy-4-oxo-1,4-dihydro­quinoline-3-carboxyl­ate monohydrate Pan, Jia Yang, Li Mao, Zhi-Hua Weng, Ling-Ling Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(16)H(17)FN(2)O(4)·H(2)O, the dihedral angle between the heterocyclic ring and the benzene ring is 5.77 (9)°, that between the heterocycle and the ethoxy­carbonyl plane is 15.5 (1)°, and that between the heterocyclic ring and the cyclopropane ring is 67.75 (13)°. In the crystal structure, mol­ecules are linked into a ribbon-like structure along the c axis by N—H⋯O and O—H⋯O hydrogen bonds. International Union of Crystallography 2008-01-30 /pmc/articles/PMC2960450/ /pubmed/21201546 http://dx.doi.org/10.1107/S1600536808002547 Text en © Pan et al. 2008 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Pan, Jia
Yang, Li
Mao, Zhi-Hua
Weng, Ling-Ling
Ethyl 7-amino-1-cyclo­propyl-6-fluoro-8-meth­oxy-4-oxo-1,4-dihydro­quinoline-3-carboxyl­ate monohydrate
title Ethyl 7-amino-1-cyclo­propyl-6-fluoro-8-meth­oxy-4-oxo-1,4-dihydro­quinoline-3-carboxyl­ate monohydrate
title_full Ethyl 7-amino-1-cyclo­propyl-6-fluoro-8-meth­oxy-4-oxo-1,4-dihydro­quinoline-3-carboxyl­ate monohydrate
title_fullStr Ethyl 7-amino-1-cyclo­propyl-6-fluoro-8-meth­oxy-4-oxo-1,4-dihydro­quinoline-3-carboxyl­ate monohydrate
title_full_unstemmed Ethyl 7-amino-1-cyclo­propyl-6-fluoro-8-meth­oxy-4-oxo-1,4-dihydro­quinoline-3-carboxyl­ate monohydrate
title_short Ethyl 7-amino-1-cyclo­propyl-6-fluoro-8-meth­oxy-4-oxo-1,4-dihydro­quinoline-3-carboxyl­ate monohydrate
title_sort ethyl 7-amino-1-cyclo­propyl-6-fluoro-8-meth­oxy-4-oxo-1,4-dihydro­quinoline-3-carboxyl­ate monohydrate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2960450/
https://www.ncbi.nlm.nih.gov/pubmed/21201546
http://dx.doi.org/10.1107/S1600536808002547
work_keys_str_mv AT panjia ethyl7amino1cyclopropyl6fluoro8methoxy4oxo14dihydroquinoline3carboxylatemonohydrate
AT yangli ethyl7amino1cyclopropyl6fluoro8methoxy4oxo14dihydroquinoline3carboxylatemonohydrate
AT maozhihua ethyl7amino1cyclopropyl6fluoro8methoxy4oxo14dihydroquinoline3carboxylatemonohydrate
AT wenglingling ethyl7amino1cyclopropyl6fluoro8methoxy4oxo14dihydroquinoline3carboxylatemonohydrate

Ejemplares similares