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N′-[4-(Dimethyl­amino)benzyl­idene]-3-hydroxy­benzohydrazide

The title compound, C(16)H(17)N(3)O(2), was synthesized by the reaction of 4-dimethyl­amino­benzaldehyde with 3-hydroxy­benzoic acid hydrazide in methanol. The dihedral angle between the two benzene rings in the mol­ecule is 9.2 (2)°. In the crystal structure, mol­ecules are linked through inter­mol...

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Detalles Bibliográficos
Autor principal: Nie, Yi
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2008
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2960467/
https://www.ncbi.nlm.nih.gov/pubmed/21201497
http://dx.doi.org/10.1107/S160053680800130X
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author Nie, Yi
author_facet Nie, Yi
author_sort Nie, Yi
collection PubMed
description The title compound, C(16)H(17)N(3)O(2), was synthesized by the reaction of 4-dimethyl­amino­benzaldehyde with 3-hydroxy­benzoic acid hydrazide in methanol. The dihedral angle between the two benzene rings in the mol­ecule is 9.2 (2)°. In the crystal structure, mol­ecules are linked through inter­molecular O—H⋯O, O—H⋯N and N—H⋯O hydrogen bonds, forming layers parallel to the bc plane.
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spelling pubmed-29604672010-12-30 N′-[4-(Dimethyl­amino)benzyl­idene]-3-hydroxy­benzohydrazide Nie, Yi Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(16)H(17)N(3)O(2), was synthesized by the reaction of 4-dimethyl­amino­benzaldehyde with 3-hydroxy­benzoic acid hydrazide in methanol. The dihedral angle between the two benzene rings in the mol­ecule is 9.2 (2)°. In the crystal structure, mol­ecules are linked through inter­molecular O—H⋯O, O—H⋯N and N—H⋯O hydrogen bonds, forming layers parallel to the bc plane. International Union of Crystallography 2008-01-18 /pmc/articles/PMC2960467/ /pubmed/21201497 http://dx.doi.org/10.1107/S160053680800130X Text en © Yi Nie 2008 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Nie, Yi
N′-[4-(Dimethyl­amino)benzyl­idene]-3-hydroxy­benzohydrazide
title N′-[4-(Dimethyl­amino)benzyl­idene]-3-hydroxy­benzohydrazide
title_full N′-[4-(Dimethyl­amino)benzyl­idene]-3-hydroxy­benzohydrazide
title_fullStr N′-[4-(Dimethyl­amino)benzyl­idene]-3-hydroxy­benzohydrazide
title_full_unstemmed N′-[4-(Dimethyl­amino)benzyl­idene]-3-hydroxy­benzohydrazide
title_short N′-[4-(Dimethyl­amino)benzyl­idene]-3-hydroxy­benzohydrazide
title_sort n′-[4-(dimethyl­amino)benzyl­idene]-3-hydroxy­benzohydrazide
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2960467/
https://www.ncbi.nlm.nih.gov/pubmed/21201497
http://dx.doi.org/10.1107/S160053680800130X
work_keys_str_mv AT nieyi n4dimethylaminobenzylidene3hydroxybenzohydrazide