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N′-(4-Hydroxybenzylidene)-4-methoxybenzohydrazide
The title compound, C(15)H(14)N(2)O(3), was prepared by the reaction of 4-hydroxybenzaldehyde and 4-methoxybenzohydrazide in methanol. The dihedral angle between the two benzene rings is 6.8 (1)°. The methoxy group is disordered over two orientations with occupancies of ca 0.63 and 0.37. In the m...
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Formato: | Texto |
Lenguaje: | English |
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International Union of Crystallography
2008
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Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2960532/ https://www.ncbi.nlm.nih.gov/pubmed/21201672 http://dx.doi.org/10.1107/S160053680802360X |
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author | Bao, Xia Wei, Yi-Jun |
author_facet | Bao, Xia Wei, Yi-Jun |
author_sort | Bao, Xia |
collection | PubMed |
description | The title compound, C(15)H(14)N(2)O(3), was prepared by the reaction of 4-hydroxybenzaldehyde and 4-methoxybenzohydrazide in methanol. The dihedral angle between the two benzene rings is 6.8 (1)°. The methoxy group is disordered over two orientations with occupancies of ca 0.63 and 0.37. In the major disorder component, the methoxy group is coplanar with the attached ring. In the crystal structure, the molecules are linked into a three-dimensional framework by intermolecular O—H⋯O and N—H⋯O hydrogen bonds. |
format | Text |
id | pubmed-2960532 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2008 |
publisher | International Union of Crystallography |
record_format | MEDLINE/PubMed |
spelling | pubmed-29605322010-12-30 N′-(4-Hydroxybenzylidene)-4-methoxybenzohydrazide Bao, Xia Wei, Yi-Jun Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(15)H(14)N(2)O(3), was prepared by the reaction of 4-hydroxybenzaldehyde and 4-methoxybenzohydrazide in methanol. The dihedral angle between the two benzene rings is 6.8 (1)°. The methoxy group is disordered over two orientations with occupancies of ca 0.63 and 0.37. In the major disorder component, the methoxy group is coplanar with the attached ring. In the crystal structure, the molecules are linked into a three-dimensional framework by intermolecular O—H⋯O and N—H⋯O hydrogen bonds. International Union of Crystallography 2008-08-06 /pmc/articles/PMC2960532/ /pubmed/21201672 http://dx.doi.org/10.1107/S160053680802360X Text en © Bao and Wei 2008 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited. |
spellingShingle | Organic Papers Bao, Xia Wei, Yi-Jun N′-(4-Hydroxybenzylidene)-4-methoxybenzohydrazide |
title |
N′-(4-Hydroxybenzylidene)-4-methoxybenzohydrazide |
title_full |
N′-(4-Hydroxybenzylidene)-4-methoxybenzohydrazide |
title_fullStr |
N′-(4-Hydroxybenzylidene)-4-methoxybenzohydrazide |
title_full_unstemmed |
N′-(4-Hydroxybenzylidene)-4-methoxybenzohydrazide |
title_short |
N′-(4-Hydroxybenzylidene)-4-methoxybenzohydrazide |
title_sort | n′-(4-hydroxybenzylidene)-4-methoxybenzohydrazide |
topic | Organic Papers |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2960532/ https://www.ncbi.nlm.nih.gov/pubmed/21201672 http://dx.doi.org/10.1107/S160053680802360X |
work_keys_str_mv | AT baoxia n4hydroxybenzylidene4methoxybenzohydrazide AT weiyijun n4hydroxybenzylidene4methoxybenzohydrazide |