2-{3-Cyano-5,5-dimethyl-4-[4-(pyrrol­idin-1-yl)buta-1,3-dien­yl]-2,5-dihydro­furan-2-yl­idene}malononitrile dichloro­methane solvate

The structure of the title compound, C(18)H(18)N(4)O·CH(2)Cl(2), was solved using data collected from a multiple crystal (note high R factors). The crystal structure is dominated by two bifurcated attractive C—H⋯N(cyano) inter­actions.

Detalles Bibliográficos
Autores principales: Gainsford, Graeme J., Bhuiyan, M. Delower H., Kay, Andrew J., Robinson, Ward T.
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2008
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2960537/
https://www.ncbi.nlm.nih.gov/pubmed/21201701
http://dx.doi.org/10.1107/S1600536808024719
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author Gainsford, Graeme J.
Bhuiyan, M. Delower H.
Kay, Andrew J.
Robinson, Ward T.
author_facet Gainsford, Graeme J.
Bhuiyan, M. Delower H.
Kay, Andrew J.
Robinson, Ward T.
author_sort Gainsford, Graeme J.
collection PubMed
description The structure of the title compound, C(18)H(18)N(4)O·CH(2)Cl(2), was solved using data collected from a multiple crystal (note high R factors). The crystal structure is dominated by two bifurcated attractive C—H⋯N(cyano) inter­actions.
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spelling pubmed-29605372010-12-30 2-{3-Cyano-5,5-dimethyl-4-[4-(pyrrol­idin-1-yl)buta-1,3-dien­yl]-2,5-dihydro­furan-2-yl­idene}malononitrile dichloro­methane solvate Gainsford, Graeme J. Bhuiyan, M. Delower H. Kay, Andrew J. Robinson, Ward T. Acta Crystallogr Sect E Struct Rep Online Organic Papers The structure of the title compound, C(18)H(18)N(4)O·CH(2)Cl(2), was solved using data collected from a multiple crystal (note high R factors). The crystal structure is dominated by two bifurcated attractive C—H⋯N(cyano) inter­actions. International Union of Crystallography 2008-08-06 /pmc/articles/PMC2960537/ /pubmed/21201701 http://dx.doi.org/10.1107/S1600536808024719 Text en © Gainsford et al. 2008 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Gainsford, Graeme J.
Bhuiyan, M. Delower H.
Kay, Andrew J.
Robinson, Ward T.
2-{3-Cyano-5,5-dimethyl-4-[4-(pyrrol­idin-1-yl)buta-1,3-dien­yl]-2,5-dihydro­furan-2-yl­idene}malononitrile dichloro­methane solvate
title 2-{3-Cyano-5,5-dimethyl-4-[4-(pyrrol­idin-1-yl)buta-1,3-dien­yl]-2,5-dihydro­furan-2-yl­idene}malononitrile dichloro­methane solvate
title_full 2-{3-Cyano-5,5-dimethyl-4-[4-(pyrrol­idin-1-yl)buta-1,3-dien­yl]-2,5-dihydro­furan-2-yl­idene}malononitrile dichloro­methane solvate
title_fullStr 2-{3-Cyano-5,5-dimethyl-4-[4-(pyrrol­idin-1-yl)buta-1,3-dien­yl]-2,5-dihydro­furan-2-yl­idene}malononitrile dichloro­methane solvate
title_full_unstemmed 2-{3-Cyano-5,5-dimethyl-4-[4-(pyrrol­idin-1-yl)buta-1,3-dien­yl]-2,5-dihydro­furan-2-yl­idene}malononitrile dichloro­methane solvate
title_short 2-{3-Cyano-5,5-dimethyl-4-[4-(pyrrol­idin-1-yl)buta-1,3-dien­yl]-2,5-dihydro­furan-2-yl­idene}malononitrile dichloro­methane solvate
title_sort 2-{3-cyano-5,5-dimethyl-4-[4-(pyrrol­idin-1-yl)buta-1,3-dien­yl]-2,5-dihydro­furan-2-yl­idene}malononitrile dichloro­methane solvate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2960537/
https://www.ncbi.nlm.nih.gov/pubmed/21201701
http://dx.doi.org/10.1107/S1600536808024719
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AT bhuiyanmdelowerh 23cyano55dimethyl44pyrrolidin1ylbuta13dienyl25dihydrofuran2ylidenemalononitriledichloromethanesolvate
AT kayandrewj 23cyano55dimethyl44pyrrolidin1ylbuta13dienyl25dihydrofuran2ylidenemalononitriledichloromethanesolvate
AT robinsonwardt 23cyano55dimethyl44pyrrolidin1ylbuta13dienyl25dihydrofuran2ylidenemalononitriledichloromethanesolvate

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