9-(4-Fluoro­phen­yl)-3,3,6,6-tetra­methyl-10-p-tolyl-1,2,3,4,5,6,7,8,9,10-deca­hydroacridine-1,8-dione

The title compound, C(30)H(32)FNO(2), was synthesized by the reaction of dimedone with 4-fluoro­benzaldehyde and p-toluidine in water. The dihydro­pyridine and both of the cyclo­hexenone rings are not planar and have flattened boat conformations. The dihedral angle between the planar aromatic rings...

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Detalles Bibliográficos
Autores principales: Tang, Ziqiang, Liu, Changning, Wu, Shanshan, Hao, Wenjuan
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2008
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2960545/
https://www.ncbi.nlm.nih.gov/pubmed/21201815
http://dx.doi.org/10.1107/S1600536808027256
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author Tang, Ziqiang
Liu, Changning
Wu, Shanshan
Hao, Wenjuan
author_facet Tang, Ziqiang
Liu, Changning
Wu, Shanshan
Hao, Wenjuan
author_sort Tang, Ziqiang
collection PubMed
description The title compound, C(30)H(32)FNO(2), was synthesized by the reaction of dimedone with 4-fluoro­benzaldehyde and p-toluidine in water. The dihydro­pyridine and both of the cyclo­hexenone rings are not planar and have flattened boat conformations. The dihedral angle between the planar aromatic rings is 15.33 (3)°. In the crystal structure, inter­molecular C—H⋯O hydrogen bonds link the mol­ecules into centrosymmetric dimers.
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spelling pubmed-29605452010-12-30 9-(4-Fluoro­phen­yl)-3,3,6,6-tetra­methyl-10-p-tolyl-1,2,3,4,5,6,7,8,9,10-deca­hydroacridine-1,8-dione Tang, Ziqiang Liu, Changning Wu, Shanshan Hao, Wenjuan Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(30)H(32)FNO(2), was synthesized by the reaction of dimedone with 4-fluoro­benzaldehyde and p-toluidine in water. The dihydro­pyridine and both of the cyclo­hexenone rings are not planar and have flattened boat conformations. The dihedral angle between the planar aromatic rings is 15.33 (3)°. In the crystal structure, inter­molecular C—H⋯O hydrogen bonds link the mol­ecules into centrosymmetric dimers. International Union of Crystallography 2008-08-30 /pmc/articles/PMC2960545/ /pubmed/21201815 http://dx.doi.org/10.1107/S1600536808027256 Text en © Tang et al. 2008 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Tang, Ziqiang
Liu, Changning
Wu, Shanshan
Hao, Wenjuan
9-(4-Fluoro­phen­yl)-3,3,6,6-tetra­methyl-10-p-tolyl-1,2,3,4,5,6,7,8,9,10-deca­hydroacridine-1,8-dione
title 9-(4-Fluoro­phen­yl)-3,3,6,6-tetra­methyl-10-p-tolyl-1,2,3,4,5,6,7,8,9,10-deca­hydroacridine-1,8-dione
title_full 9-(4-Fluoro­phen­yl)-3,3,6,6-tetra­methyl-10-p-tolyl-1,2,3,4,5,6,7,8,9,10-deca­hydroacridine-1,8-dione
title_fullStr 9-(4-Fluoro­phen­yl)-3,3,6,6-tetra­methyl-10-p-tolyl-1,2,3,4,5,6,7,8,9,10-deca­hydroacridine-1,8-dione
title_full_unstemmed 9-(4-Fluoro­phen­yl)-3,3,6,6-tetra­methyl-10-p-tolyl-1,2,3,4,5,6,7,8,9,10-deca­hydroacridine-1,8-dione
title_short 9-(4-Fluoro­phen­yl)-3,3,6,6-tetra­methyl-10-p-tolyl-1,2,3,4,5,6,7,8,9,10-deca­hydroacridine-1,8-dione
title_sort 9-(4-fluoro­phen­yl)-3,3,6,6-tetra­methyl-10-p-tolyl-1,2,3,4,5,6,7,8,9,10-deca­hydroacridine-1,8-dione
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2960545/
https://www.ncbi.nlm.nih.gov/pubmed/21201815
http://dx.doi.org/10.1107/S1600536808027256
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AT haowenjuan 94fluorophenyl3366tetramethyl10ptolyl12345678910decahydroacridine18dione

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