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Low-temperature redetermination of aqua­chloridotriphenyl­tin(IV)–1,10-phenanthroline (1/1)

The crystal structure of the title compound, [Sn(C(6)H(5))(3)Cl(H(2)O)]·C(12)H(8)N(2), which was refined in the triclinic space group P [Image: see text] [Fu, Gao, Ma & Zhang (2005 ▶). Chin. J. Synth. Chem. 13, 55–57], has been redetermined in the monoclinic space group C2/c from low-temperature...

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Autor principal: Ng, Seik Weng
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2008
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2960574/
https://www.ncbi.nlm.nih.gov/pubmed/21201582
http://dx.doi.org/10.1107/S1600536808024343
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author Ng, Seik Weng
author_facet Ng, Seik Weng
author_sort Ng, Seik Weng
collection PubMed
description The crystal structure of the title compound, [Sn(C(6)H(5))(3)Cl(H(2)O)]·C(12)H(8)N(2), which was refined in the triclinic space group P [Image: see text] [Fu, Gao, Ma & Zhang (2005 ▶). Chin. J. Synth. Chem. 13, 55–57], has been redetermined in the monoclinic space group C2/c from low-temperature diffraction measurements. The Sn atom is five-coordinate in a trans-C(3)SnClO trigonal-bipyramidal geometry; the coordinated water mol­ecule forms a pair of hydrogen bonds to the nitro­gen heterocycle.
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spelling pubmed-29605742010-12-30 Low-temperature redetermination of aqua­chloridotriphenyl­tin(IV)–1,10-phenanthroline (1/1) Ng, Seik Weng Acta Crystallogr Sect E Struct Rep Online Metal-Organic Papers The crystal structure of the title compound, [Sn(C(6)H(5))(3)Cl(H(2)O)]·C(12)H(8)N(2), which was refined in the triclinic space group P [Image: see text] [Fu, Gao, Ma & Zhang (2005 ▶). Chin. J. Synth. Chem. 13, 55–57], has been redetermined in the monoclinic space group C2/c from low-temperature diffraction measurements. The Sn atom is five-coordinate in a trans-C(3)SnClO trigonal-bipyramidal geometry; the coordinated water mol­ecule forms a pair of hydrogen bonds to the nitro­gen heterocycle. International Union of Crystallography 2008-08-06 /pmc/articles/PMC2960574/ /pubmed/21201582 http://dx.doi.org/10.1107/S1600536808024343 Text en © Seik Weng Ng 2008 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Metal-Organic Papers
Ng, Seik Weng
Low-temperature redetermination of aqua­chloridotriphenyl­tin(IV)–1,10-phenanthroline (1/1)
title Low-temperature redetermination of aqua­chloridotriphenyl­tin(IV)–1,10-phenanthroline (1/1)
title_full Low-temperature redetermination of aqua­chloridotriphenyl­tin(IV)–1,10-phenanthroline (1/1)
title_fullStr Low-temperature redetermination of aqua­chloridotriphenyl­tin(IV)–1,10-phenanthroline (1/1)
title_full_unstemmed Low-temperature redetermination of aqua­chloridotriphenyl­tin(IV)–1,10-phenanthroline (1/1)
title_short Low-temperature redetermination of aqua­chloridotriphenyl­tin(IV)–1,10-phenanthroline (1/1)
title_sort low-temperature redetermination of aqua­chloridotriphenyl­tin(iv)–1,10-phenanthroline (1/1)
topic Metal-Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2960574/
https://www.ncbi.nlm.nih.gov/pubmed/21201582
http://dx.doi.org/10.1107/S1600536808024343
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