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Low-temperature redetermination of aquachloridotriphenyltin(IV)–1,10-phenanthroline (1/1)
The crystal structure of the title compound, [Sn(C(6)H(5))(3)Cl(H(2)O)]·C(12)H(8)N(2), which was refined in the triclinic space group P [Image: see text] [Fu, Gao, Ma & Zhang (2005 ▶). Chin. J. Synth. Chem. 13, 55–57], has been redetermined in the monoclinic space group C2/c from low-temperature...
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Formato: | Texto |
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International Union of Crystallography
2008
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Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2960574/ https://www.ncbi.nlm.nih.gov/pubmed/21201582 http://dx.doi.org/10.1107/S1600536808024343 |
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author | Ng, Seik Weng |
author_facet | Ng, Seik Weng |
author_sort | Ng, Seik Weng |
collection | PubMed |
description | The crystal structure of the title compound, [Sn(C(6)H(5))(3)Cl(H(2)O)]·C(12)H(8)N(2), which was refined in the triclinic space group P [Image: see text] [Fu, Gao, Ma & Zhang (2005 ▶). Chin. J. Synth. Chem. 13, 55–57], has been redetermined in the monoclinic space group C2/c from low-temperature diffraction measurements. The Sn atom is five-coordinate in a trans-C(3)SnClO trigonal-bipyramidal geometry; the coordinated water molecule forms a pair of hydrogen bonds to the nitrogen heterocycle. |
format | Text |
id | pubmed-2960574 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2008 |
publisher | International Union of Crystallography |
record_format | MEDLINE/PubMed |
spelling | pubmed-29605742010-12-30 Low-temperature redetermination of aquachloridotriphenyltin(IV)–1,10-phenanthroline (1/1) Ng, Seik Weng Acta Crystallogr Sect E Struct Rep Online Metal-Organic Papers The crystal structure of the title compound, [Sn(C(6)H(5))(3)Cl(H(2)O)]·C(12)H(8)N(2), which was refined in the triclinic space group P [Image: see text] [Fu, Gao, Ma & Zhang (2005 ▶). Chin. J. Synth. Chem. 13, 55–57], has been redetermined in the monoclinic space group C2/c from low-temperature diffraction measurements. The Sn atom is five-coordinate in a trans-C(3)SnClO trigonal-bipyramidal geometry; the coordinated water molecule forms a pair of hydrogen bonds to the nitrogen heterocycle. International Union of Crystallography 2008-08-06 /pmc/articles/PMC2960574/ /pubmed/21201582 http://dx.doi.org/10.1107/S1600536808024343 Text en © Seik Weng Ng 2008 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited. |
spellingShingle | Metal-Organic Papers Ng, Seik Weng Low-temperature redetermination of aquachloridotriphenyltin(IV)–1,10-phenanthroline (1/1) |
title | Low-temperature redetermination of aquachloridotriphenyltin(IV)–1,10-phenanthroline (1/1) |
title_full | Low-temperature redetermination of aquachloridotriphenyltin(IV)–1,10-phenanthroline (1/1) |
title_fullStr | Low-temperature redetermination of aquachloridotriphenyltin(IV)–1,10-phenanthroline (1/1) |
title_full_unstemmed | Low-temperature redetermination of aquachloridotriphenyltin(IV)–1,10-phenanthroline (1/1) |
title_short | Low-temperature redetermination of aquachloridotriphenyltin(IV)–1,10-phenanthroline (1/1) |
title_sort | low-temperature redetermination of aquachloridotriphenyltin(iv)–1,10-phenanthroline (1/1) |
topic | Metal-Organic Papers |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2960574/ https://www.ncbi.nlm.nih.gov/pubmed/21201582 http://dx.doi.org/10.1107/S1600536808024343 |
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