1-[1-(4-Nitro­phen­yl)ethyl­idene]thio­semicarbazide

The title compound, C(9)H(10)N(4)O(2)S, was prepared by the reaction of 1-(4-nitro­phen­yl)ethanone and thio­semicarbazide in ethanol at 367 K. There are weak inter­molecular N—H⋯S and N—H⋯O hydrogen-bonding inter­actions in the crystal structure involving the amine and nitrile groups, respectively,...

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Detalles Bibliográficos
Autores principales: Wang, Jian-Gang, Jian, Fang-Fang, Ding, Yu-Feng
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2008
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2960583/
https://www.ncbi.nlm.nih.gov/pubmed/21201713
http://dx.doi.org/10.1107/S1600536808025105
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author Wang, Jian-Gang
Jian, Fang-Fang
Ding, Yu-Feng
author_facet Wang, Jian-Gang
Jian, Fang-Fang
Ding, Yu-Feng
author_sort Wang, Jian-Gang
collection PubMed
description The title compound, C(9)H(10)N(4)O(2)S, was prepared by the reaction of 1-(4-nitro­phen­yl)ethanone and thio­semicarbazide in ethanol at 367 K. There are weak inter­molecular N—H⋯S and N—H⋯O hydrogen-bonding inter­actions in the crystal structure involving the amine and nitrile groups, respectively, as donors.
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spelling pubmed-29605832010-12-30 1-[1-(4-Nitro­phen­yl)ethyl­idene]thio­semicarbazide Wang, Jian-Gang Jian, Fang-Fang Ding, Yu-Feng Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(9)H(10)N(4)O(2)S, was prepared by the reaction of 1-(4-nitro­phen­yl)ethanone and thio­semicarbazide in ethanol at 367 K. There are weak inter­molecular N—H⋯S and N—H⋯O hydrogen-bonding inter­actions in the crystal structure involving the amine and nitrile groups, respectively, as donors. International Union of Crystallography 2008-08-09 /pmc/articles/PMC2960583/ /pubmed/21201713 http://dx.doi.org/10.1107/S1600536808025105 Text en © Wang et al. 2008 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Wang, Jian-Gang
Jian, Fang-Fang
Ding, Yu-Feng
1-[1-(4-Nitro­phen­yl)ethyl­idene]thio­semicarbazide
title 1-[1-(4-Nitro­phen­yl)ethyl­idene]thio­semicarbazide
title_full 1-[1-(4-Nitro­phen­yl)ethyl­idene]thio­semicarbazide
title_fullStr 1-[1-(4-Nitro­phen­yl)ethyl­idene]thio­semicarbazide
title_full_unstemmed 1-[1-(4-Nitro­phen­yl)ethyl­idene]thio­semicarbazide
title_short 1-[1-(4-Nitro­phen­yl)ethyl­idene]thio­semicarbazide
title_sort 1-[1-(4-nitro­phen­yl)ethyl­idene]thio­semicarbazide
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2960583/
https://www.ncbi.nlm.nih.gov/pubmed/21201713
http://dx.doi.org/10.1107/S1600536808025105
work_keys_str_mv AT wangjiangang 114nitrophenylethylidenethiosemicarbazide
AT jianfangfang 114nitrophenylethylidenethiosemicarbazide
AT dingyufeng 114nitrophenylethylidenethiosemicarbazide

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