2-Acetyl­hydrazono-2-phenyl­aceto­hydrazide

The title compound, C(10)H(12)N(4)O(2), was prepared as an inter­mediate for the synthesis of metamitron. The benzene ring plane forms dihedral angles of 66.0 (1) and 3.5 (5)° with the hydrazine plane and the acetyl­imino plane, respectively. The crystal structure involves inter­molecular N—H⋯O hydr...

Descripción completa

Detalles Bibliográficos
Autores principales: Feng, Bai-Cheng, Yang, Zhi, Yi, Xu
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2008
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2960741/
https://www.ncbi.nlm.nih.gov/pubmed/21201803
http://dx.doi.org/10.1107/S160053680802624X
_version_ 1782188813172342784
author Feng, Bai-Cheng
Yang, Zhi
Yi, Xu
author_facet Feng, Bai-Cheng
Yang, Zhi
Yi, Xu
author_sort Feng, Bai-Cheng
collection PubMed
description The title compound, C(10)H(12)N(4)O(2), was prepared as an inter­mediate for the synthesis of metamitron. The benzene ring plane forms dihedral angles of 66.0 (1) and 3.5 (5)° with the hydrazine plane and the acetyl­imino plane, respectively. The crystal structure involves inter­molecular N—H⋯O hydrogen bonds.
format Text
id pubmed-2960741
institution National Center for Biotechnology Information
language English
publishDate 2008
publisher International Union of Crystallography
record_format MEDLINE/PubMed
spelling pubmed-29607412010-12-30 2-Acetyl­hydrazono-2-phenyl­aceto­hydrazide Feng, Bai-Cheng Yang, Zhi Yi, Xu Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(10)H(12)N(4)O(2), was prepared as an inter­mediate for the synthesis of metamitron. The benzene ring plane forms dihedral angles of 66.0 (1) and 3.5 (5)° with the hydrazine plane and the acetyl­imino plane, respectively. The crystal structure involves inter­molecular N—H⋯O hydrogen bonds. International Union of Crystallography 2008-08-23 /pmc/articles/PMC2960741/ /pubmed/21201803 http://dx.doi.org/10.1107/S160053680802624X Text en © Feng and Yi 2008 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Feng, Bai-Cheng
Yang, Zhi
Yi, Xu
2-Acetyl­hydrazono-2-phenyl­aceto­hydrazide
title 2-Acetyl­hydrazono-2-phenyl­aceto­hydrazide
title_full 2-Acetyl­hydrazono-2-phenyl­aceto­hydrazide
title_fullStr 2-Acetyl­hydrazono-2-phenyl­aceto­hydrazide
title_full_unstemmed 2-Acetyl­hydrazono-2-phenyl­aceto­hydrazide
title_short 2-Acetyl­hydrazono-2-phenyl­aceto­hydrazide
title_sort 2-acetyl­hydrazono-2-phenyl­aceto­hydrazide
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2960741/
https://www.ncbi.nlm.nih.gov/pubmed/21201803
http://dx.doi.org/10.1107/S160053680802624X
work_keys_str_mv AT fengbaicheng 2acetylhydrazono2phenylacetohydrazide
AT yangzhi 2acetylhydrazono2phenylacetohydrazide
AT yixu 2acetylhydrazono2phenylacetohydrazide

Ejemplares similares