N′-(4-Methoxy­benzyl­idene)-4-nitro­benzo­hydrazide methanol solvate

The title compound, C(15)H(13)N(3)O(4)·CH(4)O, was synthesized from the reaction of 4-methoxy­benzaldehyde with 4-nitro­benzohydrazide in methanol. The benzene rings of the Schiff base mol­ecule are nearly coplanar, making a dihedral angle of 7.0 (3)°. The methanol solvent mol­ecules are linked to t...

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Detalles Bibliográficos
Autores principales: Wang, Yuan-Zhi, Wang, Ming-Dong, Diao, Yun-Peng, Cai, Qian
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2008
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2960903/
https://www.ncbi.nlm.nih.gov/pubmed/21202062
http://dx.doi.org/10.1107/S1600536808005813
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author Wang, Yuan-Zhi
Wang, Ming-Dong
Diao, Yun-Peng
Cai, Qian
author_facet Wang, Yuan-Zhi
Wang, Ming-Dong
Diao, Yun-Peng
Cai, Qian
author_sort Wang, Yuan-Zhi
collection PubMed
description The title compound, C(15)H(13)N(3)O(4)·CH(4)O, was synthesized from the reaction of 4-methoxy­benzaldehyde with 4-nitro­benzohydrazide in methanol. The benzene rings of the Schiff base mol­ecule are nearly coplanar, making a dihedral angle of 7.0 (3)°. The methanol solvent mol­ecules are linked to the Schiff base mol­ecules by N—H⋯O, O—H⋯N and O—H⋯O hydrogen bonds, forming chains running parallel to the b axis.
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spelling pubmed-29609032010-12-30 N′-(4-Methoxy­benzyl­idene)-4-nitro­benzo­hydrazide methanol solvate Wang, Yuan-Zhi Wang, Ming-Dong Diao, Yun-Peng Cai, Qian Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(15)H(13)N(3)O(4)·CH(4)O, was synthesized from the reaction of 4-methoxy­benzaldehyde with 4-nitro­benzohydrazide in methanol. The benzene rings of the Schiff base mol­ecule are nearly coplanar, making a dihedral angle of 7.0 (3)°. The methanol solvent mol­ecules are linked to the Schiff base mol­ecules by N—H⋯O, O—H⋯N and O—H⋯O hydrogen bonds, forming chains running parallel to the b axis. International Union of Crystallography 2008-03-05 /pmc/articles/PMC2960903/ /pubmed/21202062 http://dx.doi.org/10.1107/S1600536808005813 Text en © Wang et al. 2008 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Wang, Yuan-Zhi
Wang, Ming-Dong
Diao, Yun-Peng
Cai, Qian
N′-(4-Methoxy­benzyl­idene)-4-nitro­benzo­hydrazide methanol solvate
title N′-(4-Methoxy­benzyl­idene)-4-nitro­benzo­hydrazide methanol solvate
title_full N′-(4-Methoxy­benzyl­idene)-4-nitro­benzo­hydrazide methanol solvate
title_fullStr N′-(4-Methoxy­benzyl­idene)-4-nitro­benzo­hydrazide methanol solvate
title_full_unstemmed N′-(4-Methoxy­benzyl­idene)-4-nitro­benzo­hydrazide methanol solvate
title_short N′-(4-Methoxy­benzyl­idene)-4-nitro­benzo­hydrazide methanol solvate
title_sort n′-(4-methoxy­benzyl­idene)-4-nitro­benzo­hydrazide methanol solvate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2960903/
https://www.ncbi.nlm.nih.gov/pubmed/21202062
http://dx.doi.org/10.1107/S1600536808005813
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AT diaoyunpeng n4methoxybenzylidene4nitrobenzohydrazidemethanolsolvate
AT caiqian n4methoxybenzylidene4nitrobenzohydrazidemethanolsolvate

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