2-(Methyl­sulfan­yl)cyclo­dodeca­none tosyl­hydrazone

The title compound, C(20)H(32)N(2)O(2)S(2), has been synthesized by the reaction of α-methyl­sulfanylcyclo­dodeca­none and p-toluene­sulfonyl­hydrazine. In the crystal structure, the conformation of the non-benzenoid ring is [3333] and the methyl­sulfanyl group is in the α-side exo position. The mol...

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Detalles Bibliográficos
Autores principales: Yan, Xiao-Jing, Liang, Xiao-Mei, Jin, Shu-Hui, Wang, Dao-Quan
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2008
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2960983/
https://www.ncbi.nlm.nih.gov/pubmed/21202054
http://dx.doi.org/10.1107/S1600536808005515
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author Yan, Xiao-Jing
Liang, Xiao-Mei
Jin, Shu-Hui
Wang, Dao-Quan
author_facet Yan, Xiao-Jing
Liang, Xiao-Mei
Jin, Shu-Hui
Wang, Dao-Quan
author_sort Yan, Xiao-Jing
collection PubMed
description The title compound, C(20)H(32)N(2)O(2)S(2), has been synthesized by the reaction of α-methyl­sulfanylcyclo­dodeca­none and p-toluene­sulfonyl­hydrazine. In the crystal structure, the conformation of the non-benzenoid ring is [3333] and the methyl­sulfanyl group is in the α-side exo position. The mol­ecules are linked by inter­molecular N—H⋯S hydrogen bonds.
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spelling pubmed-29609832010-12-30 2-(Methyl­sulfan­yl)cyclo­dodeca­none tosyl­hydrazone Yan, Xiao-Jing Liang, Xiao-Mei Jin, Shu-Hui Wang, Dao-Quan Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(20)H(32)N(2)O(2)S(2), has been synthesized by the reaction of α-methyl­sulfanylcyclo­dodeca­none and p-toluene­sulfonyl­hydrazine. In the crystal structure, the conformation of the non-benzenoid ring is [3333] and the methyl­sulfanyl group is in the α-side exo position. The mol­ecules are linked by inter­molecular N—H⋯S hydrogen bonds. International Union of Crystallography 2008-03-05 /pmc/articles/PMC2960983/ /pubmed/21202054 http://dx.doi.org/10.1107/S1600536808005515 Text en © Yan et al. 2008 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Yan, Xiao-Jing
Liang, Xiao-Mei
Jin, Shu-Hui
Wang, Dao-Quan
2-(Methyl­sulfan­yl)cyclo­dodeca­none tosyl­hydrazone
title 2-(Methyl­sulfan­yl)cyclo­dodeca­none tosyl­hydrazone
title_full 2-(Methyl­sulfan­yl)cyclo­dodeca­none tosyl­hydrazone
title_fullStr 2-(Methyl­sulfan­yl)cyclo­dodeca­none tosyl­hydrazone
title_full_unstemmed 2-(Methyl­sulfan­yl)cyclo­dodeca­none tosyl­hydrazone
title_short 2-(Methyl­sulfan­yl)cyclo­dodeca­none tosyl­hydrazone
title_sort 2-(methyl­sulfan­yl)cyclo­dodeca­none tosyl­hydrazone
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2960983/
https://www.ncbi.nlm.nih.gov/pubmed/21202054
http://dx.doi.org/10.1107/S1600536808005515
work_keys_str_mv AT yanxiaojing 2methylsulfanylcyclododecanonetosylhydrazone
AT liangxiaomei 2methylsulfanylcyclododecanonetosylhydrazone
AT jinshuhui 2methylsulfanylcyclododecanonetosylhydrazone
AT wangdaoquan 2methylsulfanylcyclododecanonetosylhydrazone

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