2-(1H-1,2,3-Benzotriazol-1-yl)-N′-cyclo­pentyl­ideneacetohydrazide

The title compound, C(13)H(15)N(5)O, was synthesized by the reaction of 2-(1H-1,2,3-benzotriazol-1-yl)acetohydrazide with cyclo­penta­none. In the cyclopentane ring, two C atoms and their attached H atoms are disordered over two positions; the site occupancy factors are ca 0.63 and 0.37. In the crys...

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Detalles Bibliográficos
Autores principales: Ji, Ning-Ning, Shi, Zhi-Qiang
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2008
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2961015/
https://www.ncbi.nlm.nih.gov/pubmed/21202052
http://dx.doi.org/10.1107/S1600536808005631
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author Ji, Ning-Ning
Shi, Zhi-Qiang
author_facet Ji, Ning-Ning
Shi, Zhi-Qiang
author_sort Ji, Ning-Ning
collection PubMed
description The title compound, C(13)H(15)N(5)O, was synthesized by the reaction of 2-(1H-1,2,3-benzotriazol-1-yl)acetohydrazide with cyclo­penta­none. In the cyclopentane ring, two C atoms and their attached H atoms are disordered over two positions; the site occupancy factors are ca 0.63 and 0.37. In the crystal structure, mol­ecules are linked into infinite chains directed along the b axis by N—H⋯O hydrogen bonds. In addition, there are weak C—H⋯O and C—H⋯N hydrogen bonds, as well as C—H⋯π-ring inter­actions in the structure.
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spelling pubmed-29610152010-12-30 2-(1H-1,2,3-Benzotriazol-1-yl)-N′-cyclo­pentyl­ideneacetohydrazide Ji, Ning-Ning Shi, Zhi-Qiang Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(13)H(15)N(5)O, was synthesized by the reaction of 2-(1H-1,2,3-benzotriazol-1-yl)acetohydrazide with cyclo­penta­none. In the cyclopentane ring, two C atoms and their attached H atoms are disordered over two positions; the site occupancy factors are ca 0.63 and 0.37. In the crystal structure, mol­ecules are linked into infinite chains directed along the b axis by N—H⋯O hydrogen bonds. In addition, there are weak C—H⋯O and C—H⋯N hydrogen bonds, as well as C—H⋯π-ring inter­actions in the structure. International Union of Crystallography 2008-03-05 /pmc/articles/PMC2961015/ /pubmed/21202052 http://dx.doi.org/10.1107/S1600536808005631 Text en © Ji and Shi 2008 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Ji, Ning-Ning
Shi, Zhi-Qiang
2-(1H-1,2,3-Benzotriazol-1-yl)-N′-cyclo­pentyl­ideneacetohydrazide
title 2-(1H-1,2,3-Benzotriazol-1-yl)-N′-cyclo­pentyl­ideneacetohydrazide
title_full 2-(1H-1,2,3-Benzotriazol-1-yl)-N′-cyclo­pentyl­ideneacetohydrazide
title_fullStr 2-(1H-1,2,3-Benzotriazol-1-yl)-N′-cyclo­pentyl­ideneacetohydrazide
title_full_unstemmed 2-(1H-1,2,3-Benzotriazol-1-yl)-N′-cyclo­pentyl­ideneacetohydrazide
title_short 2-(1H-1,2,3-Benzotriazol-1-yl)-N′-cyclo­pentyl­ideneacetohydrazide
title_sort 2-(1h-1,2,3-benzotriazol-1-yl)-n′-cyclo­pentyl­ideneacetohydrazide
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2961015/
https://www.ncbi.nlm.nih.gov/pubmed/21202052
http://dx.doi.org/10.1107/S1600536808005631
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AT shizhiqiang 21h123benzotriazol1ylncyclopentylideneacetohydrazide

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