N′-(3,5-Dichloro-2-hydroxy­benzyl­idene)-3-methoxy­benzohydrazide methanol solvate

In the title compound, C(15)H(12)Cl(2)N(2)O(3)·CH(3)OH, the Schiff base mol­ecule is nearly planar, with a dihedral angle of 4.5 (2)° between the two benzene rings. An intra­molecular O—H⋯N hydrogen bond is observed. The methanol solvent mol­ecule is linked to the Schiff base mol­ecule through inter...

Descripción completa

Detalles Bibliográficos
Autores principales: Ling, Chun-Hua, Chen, Yan-Bin, Huang, Jian-An, Ji, Cheng, Liu, Peng
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2008
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2961072/
https://www.ncbi.nlm.nih.gov/pubmed/21202428
http://dx.doi.org/10.1107/S160053680801235X
_version_ 1782188894427545600
author Ling, Chun-Hua
Chen, Yan-Bin
Huang, Jian-An
Ji, Cheng
Liu, Peng
author_facet Ling, Chun-Hua
Chen, Yan-Bin
Huang, Jian-An
Ji, Cheng
Liu, Peng
author_sort Ling, Chun-Hua
collection PubMed
description In the title compound, C(15)H(12)Cl(2)N(2)O(3)·CH(3)OH, the Schiff base mol­ecule is nearly planar, with a dihedral angle of 4.5 (2)° between the two benzene rings. An intra­molecular O—H⋯N hydrogen bond is observed. The methanol solvent mol­ecule is linked to the Schiff base mol­ecule through inter­molecular N—H⋯O and O—H⋯O hydrogen bonds.
format Text
id pubmed-2961072
institution National Center for Biotechnology Information
language English
publishDate 2008
publisher International Union of Crystallography
record_format MEDLINE/PubMed
spelling pubmed-29610722010-12-30 N′-(3,5-Dichloro-2-hydroxy­benzyl­idene)-3-methoxy­benzohydrazide methanol solvate Ling, Chun-Hua Chen, Yan-Bin Huang, Jian-An Ji, Cheng Liu, Peng Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(15)H(12)Cl(2)N(2)O(3)·CH(3)OH, the Schiff base mol­ecule is nearly planar, with a dihedral angle of 4.5 (2)° between the two benzene rings. An intra­molecular O—H⋯N hydrogen bond is observed. The methanol solvent mol­ecule is linked to the Schiff base mol­ecule through inter­molecular N—H⋯O and O—H⋯O hydrogen bonds. International Union of Crystallography 2008-04-30 /pmc/articles/PMC2961072/ /pubmed/21202428 http://dx.doi.org/10.1107/S160053680801235X Text en © Ling et al. 2008 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Ling, Chun-Hua
Chen, Yan-Bin
Huang, Jian-An
Ji, Cheng
Liu, Peng
N′-(3,5-Dichloro-2-hydroxy­benzyl­idene)-3-methoxy­benzohydrazide methanol solvate
title N′-(3,5-Dichloro-2-hydroxy­benzyl­idene)-3-methoxy­benzohydrazide methanol solvate
title_full N′-(3,5-Dichloro-2-hydroxy­benzyl­idene)-3-methoxy­benzohydrazide methanol solvate
title_fullStr N′-(3,5-Dichloro-2-hydroxy­benzyl­idene)-3-methoxy­benzohydrazide methanol solvate
title_full_unstemmed N′-(3,5-Dichloro-2-hydroxy­benzyl­idene)-3-methoxy­benzohydrazide methanol solvate
title_short N′-(3,5-Dichloro-2-hydroxy­benzyl­idene)-3-methoxy­benzohydrazide methanol solvate
title_sort n′-(3,5-dichloro-2-hydroxy­benzyl­idene)-3-methoxy­benzohydrazide methanol solvate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2961072/
https://www.ncbi.nlm.nih.gov/pubmed/21202428
http://dx.doi.org/10.1107/S160053680801235X
work_keys_str_mv AT lingchunhua n35dichloro2hydroxybenzylidene3methoxybenzohydrazidemethanolsolvate
AT chenyanbin n35dichloro2hydroxybenzylidene3methoxybenzohydrazidemethanolsolvate
AT huangjianan n35dichloro2hydroxybenzylidene3methoxybenzohydrazidemethanolsolvate
AT jicheng n35dichloro2hydroxybenzylidene3methoxybenzohydrazidemethanolsolvate
AT liupeng n35dichloro2hydroxybenzylidene3methoxybenzohydrazidemethanolsolvate

Ejemplares similares