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4-(Diethylamino)salicylaldehyde phenylsulfonylhydrazone
In the title compound, C(17)H(21)N(3)O(3)S, the dihedral angle between the aromatic ring planes is 84.2 (2)°. The pendant ethyl groups of the –N(C(2)H(5))(2) group are disordered over two sets of positions in a 0.84 (2):0.16 (2) ratio. The molecular conformation is stabilized by an intramolecular...
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Formato: | Texto |
Lenguaje: | English |
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International Union of Crystallography
2008
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Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2961088/ https://www.ncbi.nlm.nih.gov/pubmed/21202352 http://dx.doi.org/10.1107/S1600536808010118 |
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author | Tai, Xi-Shi Feng, Yi-Min Kong, Fan-Yuan |
author_facet | Tai, Xi-Shi Feng, Yi-Min Kong, Fan-Yuan |
author_sort | Tai, Xi-Shi |
collection | PubMed |
description | In the title compound, C(17)H(21)N(3)O(3)S, the dihedral angle between the aromatic ring planes is 84.2 (2)°. The pendant ethyl groups of the –N(C(2)H(5))(2) group are disordered over two sets of positions in a 0.84 (2):0.16 (2) ratio. The molecular conformation is stabilized by an intramolecular O—H⋯N hydrogen bond, and intermolecular N—H⋯O bonds lead to [010] chains in the crystal structure. |
format | Text |
id | pubmed-2961088 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2008 |
publisher | International Union of Crystallography |
record_format | MEDLINE/PubMed |
spelling | pubmed-29610882010-12-30 4-(Diethylamino)salicylaldehyde phenylsulfonylhydrazone Tai, Xi-Shi Feng, Yi-Min Kong, Fan-Yuan Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(17)H(21)N(3)O(3)S, the dihedral angle between the aromatic ring planes is 84.2 (2)°. The pendant ethyl groups of the –N(C(2)H(5))(2) group are disordered over two sets of positions in a 0.84 (2):0.16 (2) ratio. The molecular conformation is stabilized by an intramolecular O—H⋯N hydrogen bond, and intermolecular N—H⋯O bonds lead to [010] chains in the crystal structure. International Union of Crystallography 2008-04-18 /pmc/articles/PMC2961088/ /pubmed/21202352 http://dx.doi.org/10.1107/S1600536808010118 Text en © Tai et al. 2008 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited. |
spellingShingle | Organic Papers Tai, Xi-Shi Feng, Yi-Min Kong, Fan-Yuan 4-(Diethylamino)salicylaldehyde phenylsulfonylhydrazone |
title | 4-(Diethylamino)salicylaldehyde phenylsulfonylhydrazone |
title_full | 4-(Diethylamino)salicylaldehyde phenylsulfonylhydrazone |
title_fullStr | 4-(Diethylamino)salicylaldehyde phenylsulfonylhydrazone |
title_full_unstemmed | 4-(Diethylamino)salicylaldehyde phenylsulfonylhydrazone |
title_short | 4-(Diethylamino)salicylaldehyde phenylsulfonylhydrazone |
title_sort | 4-(diethylamino)salicylaldehyde phenylsulfonylhydrazone |
topic | Organic Papers |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2961088/ https://www.ncbi.nlm.nih.gov/pubmed/21202352 http://dx.doi.org/10.1107/S1600536808010118 |
work_keys_str_mv | AT taixishi 4diethylaminosalicylaldehydephenylsulfonylhydrazone AT fengyimin 4diethylaminosalicylaldehydephenylsulfonylhydrazone AT kongfanyuan 4diethylaminosalicylaldehydephenylsulfonylhydrazone |