Low-temperature redetermination of 3,4,5,6-tetra­hydro­pyrimidin-2(1H)-one

The low-temperature structure of the title compound, C(4)H(8)N(2)O, is ordered, whereas the central methyl­ene groups is disordered in the reported room-temperature structure. The molecule lies across a mirror plane; adjacent mol­ecules are linked by an N—H⋯O hydrogen bond into a chain.

Detalles Bibliográficos
Autores principales: Rizal, Mohd. Razali, Azizul, Isha, Ng, Seik Weng
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2008
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2961143/
https://www.ncbi.nlm.nih.gov/pubmed/21202396
http://dx.doi.org/10.1107/S160053680801115X
_version_ 1782188911969173504
author Rizal, Mohd. Razali
Azizul, Isha
Ng, Seik Weng
author_facet Rizal, Mohd. Razali
Azizul, Isha
Ng, Seik Weng
author_sort Rizal, Mohd. Razali
collection PubMed
description The low-temperature structure of the title compound, C(4)H(8)N(2)O, is ordered, whereas the central methyl­ene groups is disordered in the reported room-temperature structure. The molecule lies across a mirror plane; adjacent mol­ecules are linked by an N—H⋯O hydrogen bond into a chain.
format Text
id pubmed-2961143
institution National Center for Biotechnology Information
language English
publishDate 2008
publisher International Union of Crystallography
record_format MEDLINE/PubMed
spelling pubmed-29611432010-12-30 Low-temperature redetermination of 3,4,5,6-tetra­hydro­pyrimidin-2(1H)-one Rizal, Mohd. Razali Azizul, Isha Ng, Seik Weng Acta Crystallogr Sect E Struct Rep Online Organic Papers The low-temperature structure of the title compound, C(4)H(8)N(2)O, is ordered, whereas the central methyl­ene groups is disordered in the reported room-temperature structure. The molecule lies across a mirror plane; adjacent mol­ecules are linked by an N—H⋯O hydrogen bond into a chain. International Union of Crystallography 2008-04-26 /pmc/articles/PMC2961143/ /pubmed/21202396 http://dx.doi.org/10.1107/S160053680801115X Text en © Rizal et al. 2008 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Rizal, Mohd. Razali
Azizul, Isha
Ng, Seik Weng
Low-temperature redetermination of 3,4,5,6-tetra­hydro­pyrimidin-2(1H)-one
title Low-temperature redetermination of 3,4,5,6-tetra­hydro­pyrimidin-2(1H)-one
title_full Low-temperature redetermination of 3,4,5,6-tetra­hydro­pyrimidin-2(1H)-one
title_fullStr Low-temperature redetermination of 3,4,5,6-tetra­hydro­pyrimidin-2(1H)-one
title_full_unstemmed Low-temperature redetermination of 3,4,5,6-tetra­hydro­pyrimidin-2(1H)-one
title_short Low-temperature redetermination of 3,4,5,6-tetra­hydro­pyrimidin-2(1H)-one
title_sort low-temperature redetermination of 3,4,5,6-tetra­hydro­pyrimidin-2(1h)-one
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2961143/
https://www.ncbi.nlm.nih.gov/pubmed/21202396
http://dx.doi.org/10.1107/S160053680801115X
work_keys_str_mv AT rizalmohdrazali lowtemperatureredeterminationof3456tetrahydropyrimidin21hone
AT azizulisha lowtemperatureredeterminationof3456tetrahydropyrimidin21hone
AT ngseikweng lowtemperatureredeterminationof3456tetrahydropyrimidin21hone

Ejemplares similares