2,6-Bis(3-phenyl-1H-pyrazol-5-yl)pyridine monohydrate

In the title compound, C(23)H(17)N(5)·H(2)O, the pyrazole rings are slightly twisted from the central pyridine ring, forming dihedral angles of 5.3 (2) and 3.5 (2)°. The pyrazole and phenyl rings on each side of the pyridine ring are also approximately coplanar, making dihedral angles of 6.0 (2) and...

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Detalles Bibliográficos
Autores principales: Dong, Jian-Yu, You, Tian-Pa
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2008
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2961158/
https://www.ncbi.nlm.nih.gov/pubmed/21202310
http://dx.doi.org/10.1107/S1600536808008520
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author Dong, Jian-Yu
You, Tian-Pa
author_facet Dong, Jian-Yu
You, Tian-Pa
author_sort Dong, Jian-Yu
collection PubMed
description In the title compound, C(23)H(17)N(5)·H(2)O, the pyrazole rings are slightly twisted from the central pyridine ring, forming dihedral angles of 5.3 (2) and 3.5 (2)°. The pyrazole and phenyl rings on each side of the pyridine ring are also approximately coplanar, making dihedral angles of 6.0 (2) and 4.5 (2)°. In the crystal structure, 2,6-bis­(3-phenyl-1H-pyrazol-5-yl)pyridine and water mol­ecules are linked together via N—H⋯O and O—H⋯N hydrogen bonds, forming a column running parallel to the a axis.
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spelling pubmed-29611582010-12-30 2,6-Bis(3-phenyl-1H-pyrazol-5-yl)pyridine monohydrate Dong, Jian-Yu You, Tian-Pa Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(23)H(17)N(5)·H(2)O, the pyrazole rings are slightly twisted from the central pyridine ring, forming dihedral angles of 5.3 (2) and 3.5 (2)°. The pyrazole and phenyl rings on each side of the pyridine ring are also approximately coplanar, making dihedral angles of 6.0 (2) and 4.5 (2)°. In the crystal structure, 2,6-bis­(3-phenyl-1H-pyrazol-5-yl)pyridine and water mol­ecules are linked together via N—H⋯O and O—H⋯N hydrogen bonds, forming a column running parallel to the a axis. International Union of Crystallography 2008-04-10 /pmc/articles/PMC2961158/ /pubmed/21202310 http://dx.doi.org/10.1107/S1600536808008520 Text en © Dong and You 2008 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Dong, Jian-Yu
You, Tian-Pa
2,6-Bis(3-phenyl-1H-pyrazol-5-yl)pyridine monohydrate
title 2,6-Bis(3-phenyl-1H-pyrazol-5-yl)pyridine monohydrate
title_full 2,6-Bis(3-phenyl-1H-pyrazol-5-yl)pyridine monohydrate
title_fullStr 2,6-Bis(3-phenyl-1H-pyrazol-5-yl)pyridine monohydrate
title_full_unstemmed 2,6-Bis(3-phenyl-1H-pyrazol-5-yl)pyridine monohydrate
title_short 2,6-Bis(3-phenyl-1H-pyrazol-5-yl)pyridine monohydrate
title_sort 2,6-bis(3-phenyl-1h-pyrazol-5-yl)pyridine monohydrate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2961158/
https://www.ncbi.nlm.nih.gov/pubmed/21202310
http://dx.doi.org/10.1107/S1600536808008520
work_keys_str_mv AT dongjianyu 26bis3phenyl1hpyrazol5ylpyridinemonohydrate
AT youtianpa 26bis3phenyl1hpyrazol5ylpyridinemonohydrate

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