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3-(3-Chloropropyl)-7,8-dimethoxy-2,3,4,5-tetrahydro-1H-3-benzazepin-2-one at 125 K
In the title compound, C(15)H(20)ClNO(3), the seven-membered ring adopts a distorted boat–sofa conformation; the methylene C atoms of this ring are coplanar with the benzene ring. Both methoxy groups are almost coplanar with the attached benzene ring [C—C—O—C = 6.5 (2) and −13.5 (3)°]. An intramo...
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Formato: | Texto |
Lenguaje: | English |
Publicado: |
International Union of Crystallography
2008
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2961196/ https://www.ncbi.nlm.nih.gov/pubmed/21202294 http://dx.doi.org/10.1107/S1600536808008787 |
Sumario: | In the title compound, C(15)H(20)ClNO(3), the seven-membered ring adopts a distorted boat–sofa conformation; the methylene C atoms of this ring are coplanar with the benzene ring. Both methoxy groups are almost coplanar with the attached benzene ring [C—C—O—C = 6.5 (2) and −13.5 (3)°]. An intramolecular C—H⋯O hydrogen bond is observed in the molecular structure. In the crystal structure, a C—H⋯π interaction involving the benzene ring is observed. |
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