1,6,6-Trimethyl-1H-chromeno[6,7-d]thia­zol-2(6H)-one

The title compound, C(13)H(13)NO(2)S, was prepared by a thermocyclization reaction from 3-methyl-6-(2-methyl­but-3-yn-2-yl­oxy)benzo[d]thia­zol-2(3H)-one. In the crystal structure, the methyl­thia­zole unit is planar, while the pyran ring assumes a screw-boat conformation. Intra­molecular C—H⋯O hydr...

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Detalles Bibliográficos
Autores principales: Tang, Jian, Wang, Yang, Zhang, Bei-Na, Xia, Peng
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2008
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2961216/
https://www.ncbi.nlm.nih.gov/pubmed/21202374
http://dx.doi.org/10.1107/S1600536808010623
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author Tang, Jian
Wang, Yang
Zhang, Bei-Na
Xia, Peng
author_facet Tang, Jian
Wang, Yang
Zhang, Bei-Na
Xia, Peng
author_sort Tang, Jian
collection PubMed
description The title compound, C(13)H(13)NO(2)S, was prepared by a thermocyclization reaction from 3-methyl-6-(2-methyl­but-3-yn-2-yl­oxy)benzo[d]thia­zol-2(3H)-one. In the crystal structure, the methyl­thia­zole unit is planar, while the pyran ring assumes a screw-boat conformation. Intra­molecular C—H⋯O hydrogen bonding helps to stabilize the molecular structure.
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spelling pubmed-29612162010-12-30 1,6,6-Trimethyl-1H-chromeno[6,7-d]thia­zol-2(6H)-one Tang, Jian Wang, Yang Zhang, Bei-Na Xia, Peng Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(13)H(13)NO(2)S, was prepared by a thermocyclization reaction from 3-methyl-6-(2-methyl­but-3-yn-2-yl­oxy)benzo[d]thia­zol-2(3H)-one. In the crystal structure, the methyl­thia­zole unit is planar, while the pyran ring assumes a screw-boat conformation. Intra­molecular C—H⋯O hydrogen bonding helps to stabilize the molecular structure. International Union of Crystallography 2008-04-23 /pmc/articles/PMC2961216/ /pubmed/21202374 http://dx.doi.org/10.1107/S1600536808010623 Text en © Tang et al. 2008 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Tang, Jian
Wang, Yang
Zhang, Bei-Na
Xia, Peng
1,6,6-Trimethyl-1H-chromeno[6,7-d]thia­zol-2(6H)-one
title 1,6,6-Trimethyl-1H-chromeno[6,7-d]thia­zol-2(6H)-one
title_full 1,6,6-Trimethyl-1H-chromeno[6,7-d]thia­zol-2(6H)-one
title_fullStr 1,6,6-Trimethyl-1H-chromeno[6,7-d]thia­zol-2(6H)-one
title_full_unstemmed 1,6,6-Trimethyl-1H-chromeno[6,7-d]thia­zol-2(6H)-one
title_short 1,6,6-Trimethyl-1H-chromeno[6,7-d]thia­zol-2(6H)-one
title_sort 1,6,6-trimethyl-1h-chromeno[6,7-d]thia­zol-2(6h)-one
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2961216/
https://www.ncbi.nlm.nih.gov/pubmed/21202374
http://dx.doi.org/10.1107/S1600536808010623
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AT xiapeng 166trimethyl1hchromeno67dthiazol26hone

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