5-Butyl­amino-6-(4-fluoro­phen­yl)-7-oxo-1-p-tolyl-6,7-dihydro-1H-pyrazolo[4,3-d]pyrimidine-3-carbonitrile

In the title compound, C(23)H(21)FN(6)O, the dihedral angle between the fluoro­phenyl and pyrimidinone rings is 75.9 (1)°, and the dihedral angle between the methyl­phenyl and pyrazole rings is 40.3 (1)°. In the crystal structure, weak C—H⋯π(arene) and C—N⋯π(arene) inter­actions and intermolecular C...

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Detalles Bibliográficos
Autores principales: Hu, Ji-Huan, Wu, Ming-Hu
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2008
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2961236/
https://www.ncbi.nlm.nih.gov/pubmed/21202333
http://dx.doi.org/10.1107/S1600536808009744
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author Hu, Ji-Huan
Wu, Ming-Hu
author_facet Hu, Ji-Huan
Wu, Ming-Hu
author_sort Hu, Ji-Huan
collection PubMed
description In the title compound, C(23)H(21)FN(6)O, the dihedral angle between the fluoro­phenyl and pyrimidinone rings is 75.9 (1)°, and the dihedral angle between the methyl­phenyl and pyrazole rings is 40.3 (1)°. In the crystal structure, weak C—H⋯π(arene) and C—N⋯π(arene) inter­actions and intermolecular C—H⋯N and N—H⋯O hydrogen-bonding inter­actions are present.
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spelling pubmed-29612362010-12-30 5-Butyl­amino-6-(4-fluoro­phen­yl)-7-oxo-1-p-tolyl-6,7-dihydro-1H-pyrazolo[4,3-d]pyrimidine-3-carbonitrile Hu, Ji-Huan Wu, Ming-Hu Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(23)H(21)FN(6)O, the dihedral angle between the fluoro­phenyl and pyrimidinone rings is 75.9 (1)°, and the dihedral angle between the methyl­phenyl and pyrazole rings is 40.3 (1)°. In the crystal structure, weak C—H⋯π(arene) and C—N⋯π(arene) inter­actions and intermolecular C—H⋯N and N—H⋯O hydrogen-bonding inter­actions are present. International Union of Crystallography 2008-04-16 /pmc/articles/PMC2961236/ /pubmed/21202333 http://dx.doi.org/10.1107/S1600536808009744 Text en © Hu and Wu 2008 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Hu, Ji-Huan
Wu, Ming-Hu
5-Butyl­amino-6-(4-fluoro­phen­yl)-7-oxo-1-p-tolyl-6,7-dihydro-1H-pyrazolo[4,3-d]pyrimidine-3-carbonitrile
title 5-Butyl­amino-6-(4-fluoro­phen­yl)-7-oxo-1-p-tolyl-6,7-dihydro-1H-pyrazolo[4,3-d]pyrimidine-3-carbonitrile
title_full 5-Butyl­amino-6-(4-fluoro­phen­yl)-7-oxo-1-p-tolyl-6,7-dihydro-1H-pyrazolo[4,3-d]pyrimidine-3-carbonitrile
title_fullStr 5-Butyl­amino-6-(4-fluoro­phen­yl)-7-oxo-1-p-tolyl-6,7-dihydro-1H-pyrazolo[4,3-d]pyrimidine-3-carbonitrile
title_full_unstemmed 5-Butyl­amino-6-(4-fluoro­phen­yl)-7-oxo-1-p-tolyl-6,7-dihydro-1H-pyrazolo[4,3-d]pyrimidine-3-carbonitrile
title_short 5-Butyl­amino-6-(4-fluoro­phen­yl)-7-oxo-1-p-tolyl-6,7-dihydro-1H-pyrazolo[4,3-d]pyrimidine-3-carbonitrile
title_sort 5-butyl­amino-6-(4-fluoro­phen­yl)-7-oxo-1-p-tolyl-6,7-dihydro-1h-pyrazolo[4,3-d]pyrimidine-3-carbonitrile
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2961236/
https://www.ncbi.nlm.nih.gov/pubmed/21202333
http://dx.doi.org/10.1107/S1600536808009744
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AT wuminghu 5butylamino64fluorophenyl7oxo1ptolyl67dihydro1hpyrazolo43dpyrimidine3carbonitrile

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