Cargando…

2-(2,4-Dichloro­phen­yl)-3-[5-(4-methoxy­phen­yl)-1,3,4-thia­diazol-2-yl]-1,3-thia­zolidin-4-one

In the mol­ecule of the title compound, C(18)H(13)Cl(2)N(3)O(2)S(2), the thia­zolidinone ring has an envelope conformation with the S atom displaced by 0.394 (3) Å from the plane of the other ring atoms. The thia­diazole ring is oriented at a dihedral angle of 7.40 (4)° with respect to the 4-methoxy...

Descripción completa

Detalles Bibliográficos
Autores principales: Wan, Rong, Yin, Li-He, Han, Feng, Wang, Bin, Wang, Jin-Tang
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2008
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2961251/
https://www.ncbi.nlm.nih.gov/pubmed/21202287
http://dx.doi.org/10.1107/S1600536808008465
_version_ 1782188937788260352
author Wan, Rong
Yin, Li-He
Han, Feng
Wang, Bin
Wang, Jin-Tang
author_facet Wan, Rong
Yin, Li-He
Han, Feng
Wang, Bin
Wang, Jin-Tang
author_sort Wan, Rong
collection PubMed
description In the mol­ecule of the title compound, C(18)H(13)Cl(2)N(3)O(2)S(2), the thia­zolidinone ring has an envelope conformation with the S atom displaced by 0.394 (3) Å from the plane of the other ring atoms. The thia­diazole ring is oriented at a dihedral angle of 7.40 (4)° with respect to the 4-methoxy­phenyl ring. Intra­molecular C—H⋯S, C—H⋯N and C—H⋯Cl hydrogen bonds result in the formation of two planar and two non-planar five-membered rings. The planar five-membered rings are oriented at a dihedral angle of 6.23 (3)°. The 2,4-dichloro­phenyl ring is oriented at dihedral angles of 84.21 (4) and 83.55 (3)° with respect to the thia­diazole and 4-methoxy­phenyl rings, respectively. In the crystal structure, inter­molecular C—H⋯O hydrogen bonds link the mol­ecules into centrosymmetric dimers.
format Text
id pubmed-2961251
institution National Center for Biotechnology Information
language English
publishDate 2008
publisher International Union of Crystallography
record_format MEDLINE/PubMed
spelling pubmed-29612512010-12-30 2-(2,4-Dichloro­phen­yl)-3-[5-(4-methoxy­phen­yl)-1,3,4-thia­diazol-2-yl]-1,3-thia­zolidin-4-one Wan, Rong Yin, Li-He Han, Feng Wang, Bin Wang, Jin-Tang Acta Crystallogr Sect E Struct Rep Online Organic Papers In the mol­ecule of the title compound, C(18)H(13)Cl(2)N(3)O(2)S(2), the thia­zolidinone ring has an envelope conformation with the S atom displaced by 0.394 (3) Å from the plane of the other ring atoms. The thia­diazole ring is oriented at a dihedral angle of 7.40 (4)° with respect to the 4-methoxy­phenyl ring. Intra­molecular C—H⋯S, C—H⋯N and C—H⋯Cl hydrogen bonds result in the formation of two planar and two non-planar five-membered rings. The planar five-membered rings are oriented at a dihedral angle of 6.23 (3)°. The 2,4-dichloro­phenyl ring is oriented at dihedral angles of 84.21 (4) and 83.55 (3)° with respect to the thia­diazole and 4-methoxy­phenyl rings, respectively. In the crystal structure, inter­molecular C—H⋯O hydrogen bonds link the mol­ecules into centrosymmetric dimers. International Union of Crystallography 2008-04-04 /pmc/articles/PMC2961251/ /pubmed/21202287 http://dx.doi.org/10.1107/S1600536808008465 Text en © Wan et al. 2008 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Wan, Rong
Yin, Li-He
Han, Feng
Wang, Bin
Wang, Jin-Tang
2-(2,4-Dichloro­phen­yl)-3-[5-(4-methoxy­phen­yl)-1,3,4-thia­diazol-2-yl]-1,3-thia­zolidin-4-one
title 2-(2,4-Dichloro­phen­yl)-3-[5-(4-methoxy­phen­yl)-1,3,4-thia­diazol-2-yl]-1,3-thia­zolidin-4-one
title_full 2-(2,4-Dichloro­phen­yl)-3-[5-(4-methoxy­phen­yl)-1,3,4-thia­diazol-2-yl]-1,3-thia­zolidin-4-one
title_fullStr 2-(2,4-Dichloro­phen­yl)-3-[5-(4-methoxy­phen­yl)-1,3,4-thia­diazol-2-yl]-1,3-thia­zolidin-4-one
title_full_unstemmed 2-(2,4-Dichloro­phen­yl)-3-[5-(4-methoxy­phen­yl)-1,3,4-thia­diazol-2-yl]-1,3-thia­zolidin-4-one
title_short 2-(2,4-Dichloro­phen­yl)-3-[5-(4-methoxy­phen­yl)-1,3,4-thia­diazol-2-yl]-1,3-thia­zolidin-4-one
title_sort 2-(2,4-dichloro­phen­yl)-3-[5-(4-methoxy­phen­yl)-1,3,4-thia­diazol-2-yl]-1,3-thia­zolidin-4-one
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2961251/
https://www.ncbi.nlm.nih.gov/pubmed/21202287
http://dx.doi.org/10.1107/S1600536808008465
work_keys_str_mv AT wanrong 224dichlorophenyl354methoxyphenyl134thiadiazol2yl13thiazolidin4one
AT yinlihe 224dichlorophenyl354methoxyphenyl134thiadiazol2yl13thiazolidin4one
AT hanfeng 224dichlorophenyl354methoxyphenyl134thiadiazol2yl13thiazolidin4one
AT wangbin 224dichlorophenyl354methoxyphenyl134thiadiazol2yl13thiazolidin4one
AT wangjintang 224dichlorophenyl354methoxyphenyl134thiadiazol2yl13thiazolidin4one