Bis[4-(dimethyl­amino)phen­yl]diazene oxide

The asymmetric unit of the title compound, C(16)H(20)N(4)O, contains six independent approximately planar mol­ecules and is best described as a commensurate modulation of a P2(1)/c parent. Two sets of disordered mol­ecules share almost the same locations (related by an in-plane translation), ensurin...

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Detalles Bibliográficos
Autores principales: Gainsford, Graeme J., Bhuiyan, M. Delower H., Kay, Andrew J.
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2008
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2961315/
https://www.ncbi.nlm.nih.gov/pubmed/21202360
http://dx.doi.org/10.1107/S1600536808006740
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author Gainsford, Graeme J.
Bhuiyan, M. Delower H.
Kay, Andrew J.
author_facet Gainsford, Graeme J.
Bhuiyan, M. Delower H.
Kay, Andrew J.
author_sort Gainsford, Graeme J.
collection PubMed
description The asymmetric unit of the title compound, C(16)H(20)N(4)O, contains six independent approximately planar mol­ecules and is best described as a commensurate modulation of a P2(1)/c parent. Two sets of disordered mol­ecules share almost the same locations (related by an in-plane translation), ensuring that the c-glide plane condition is not attained. C—H⋯O inter­actions provide structural cohesion. The site occupancy factors of the disordered molecules are ca 0.72/0.28 and 0.67/0.33.
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spelling pubmed-29613152010-12-30 Bis[4-(dimethyl­amino)phen­yl]diazene oxide Gainsford, Graeme J. Bhuiyan, M. Delower H. Kay, Andrew J. Acta Crystallogr Sect E Struct Rep Online Organic Papers The asymmetric unit of the title compound, C(16)H(20)N(4)O, contains six independent approximately planar mol­ecules and is best described as a commensurate modulation of a P2(1)/c parent. Two sets of disordered mol­ecules share almost the same locations (related by an in-plane translation), ensuring that the c-glide plane condition is not attained. C—H⋯O inter­actions provide structural cohesion. The site occupancy factors of the disordered molecules are ca 0.72/0.28 and 0.67/0.33. International Union of Crystallography 2008-04-18 /pmc/articles/PMC2961315/ /pubmed/21202360 http://dx.doi.org/10.1107/S1600536808006740 Text en © Gainsford et al. 2008 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Gainsford, Graeme J.
Bhuiyan, M. Delower H.
Kay, Andrew J.
Bis[4-(dimethyl­amino)phen­yl]diazene oxide
title Bis[4-(dimethyl­amino)phen­yl]diazene oxide
title_full Bis[4-(dimethyl­amino)phen­yl]diazene oxide
title_fullStr Bis[4-(dimethyl­amino)phen­yl]diazene oxide
title_full_unstemmed Bis[4-(dimethyl­amino)phen­yl]diazene oxide
title_short Bis[4-(dimethyl­amino)phen­yl]diazene oxide
title_sort bis[4-(dimethyl­amino)phen­yl]diazene oxide
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2961315/
https://www.ncbi.nlm.nih.gov/pubmed/21202360
http://dx.doi.org/10.1107/S1600536808006740
work_keys_str_mv AT gainsfordgraemej bis4dimethylaminophenyldiazeneoxide
AT bhuiyanmdelowerh bis4dimethylaminophenyldiazeneoxide
AT kayandrewj bis4dimethylaminophenyldiazeneoxide

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