1,2-Bis(N′-benzoyl­thio­ureido)benzene

The title compound, C(22)H(18)N(4)O(2)S(2), was characterized by (1)H and (13)C NMR, solid-state IR spectroscopy and X-ray crystallographic techniques. The crystal structure determination reveals that the twisting modes of the two side arms are different [C—N—C—O and C—N—C—N torsion angles = −1.2 (3...

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Detalles Bibliográficos
Autores principales: Thiam, Elhadj Ibrahima, Diop, Mayoro, Gaye, Mohamed, Sall, Abdou Salam, Barry, Aliou Hamady
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2008
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2961338/
https://www.ncbi.nlm.nih.gov/pubmed/21202269
http://dx.doi.org/10.1107/S1600536808008374
Descripción
Sumario:The title compound, C(22)H(18)N(4)O(2)S(2), was characterized by (1)H and (13)C NMR, solid-state IR spectroscopy and X-ray crystallographic techniques. The crystal structure determination reveals that the twisting modes of the two side arms are different [C—N—C—O and C—N—C—N torsion angles = −1.2 (3) and 1.1 (3)°, respectively, in one arm and 24.1 (3) and −5.1 (3)°, respectively, in the other]. The crystal structure involves N—H⋯O and N—H⋯S hydrogen bonds.

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