4-Acetyl-2,3,4,5-tetra­hydro-1H-1,4-benzodiazepine

The title compound, C(11)H(14)N(2)O·H(2)O, crystallizes with one formula unit in the asymmetric unit. The seven-membered ring has a chair conformation with the C=O group turned away from the benzene ring. N—H⋯O and O—H⋯O hydrogen bonds are present in the crystal structure.

Detalles Bibliográficos
Autores principales: Zhao, Qing-Jie, Liu, Zheng, Zheng, Jin, Shen, Jing-Shan
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2008
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2961359/
https://www.ncbi.nlm.nih.gov/pubmed/21202698
http://dx.doi.org/10.1107/S1600536808007927
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author Zhao, Qing-Jie
Liu, Zheng
Zheng, Jin
Shen, Jing-Shan
author_facet Zhao, Qing-Jie
Liu, Zheng
Zheng, Jin
Shen, Jing-Shan
author_sort Zhao, Qing-Jie
collection PubMed
description The title compound, C(11)H(14)N(2)O·H(2)O, crystallizes with one formula unit in the asymmetric unit. The seven-membered ring has a chair conformation with the C=O group turned away from the benzene ring. N—H⋯O and O—H⋯O hydrogen bonds are present in the crystal structure.
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spelling pubmed-29613592010-12-30 4-Acetyl-2,3,4,5-tetra­hydro-1H-1,4-benzodiazepine Zhao, Qing-Jie Liu, Zheng Zheng, Jin Shen, Jing-Shan Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(11)H(14)N(2)O·H(2)O, crystallizes with one formula unit in the asymmetric unit. The seven-membered ring has a chair conformation with the C=O group turned away from the benzene ring. N—H⋯O and O—H⋯O hydrogen bonds are present in the crystal structure. International Union of Crystallography 2008-05-03 /pmc/articles/PMC2961359/ /pubmed/21202698 http://dx.doi.org/10.1107/S1600536808007927 Text en © Zhao et al. 2008 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Zhao, Qing-Jie
Liu, Zheng
Zheng, Jin
Shen, Jing-Shan
4-Acetyl-2,3,4,5-tetra­hydro-1H-1,4-benzodiazepine
title 4-Acetyl-2,3,4,5-tetra­hydro-1H-1,4-benzodiazepine
title_full 4-Acetyl-2,3,4,5-tetra­hydro-1H-1,4-benzodiazepine
title_fullStr 4-Acetyl-2,3,4,5-tetra­hydro-1H-1,4-benzodiazepine
title_full_unstemmed 4-Acetyl-2,3,4,5-tetra­hydro-1H-1,4-benzodiazepine
title_short 4-Acetyl-2,3,4,5-tetra­hydro-1H-1,4-benzodiazepine
title_sort 4-acetyl-2,3,4,5-tetra­hydro-1h-1,4-benzodiazepine
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2961359/
https://www.ncbi.nlm.nih.gov/pubmed/21202698
http://dx.doi.org/10.1107/S1600536808007927
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AT liuzheng 4acetyl2345tetrahydro1h14benzodiazepine
AT zhengjin 4acetyl2345tetrahydro1h14benzodiazepine
AT shenjingshan 4acetyl2345tetrahydro1h14benzodiazepine

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