(E)-2-Hydr­oxy-3-methoxy­benzaldehyde thio­semicarbazone

In the title compound, C(9)H(11)N(3)O(2)S, intra­molecular O—H⋯O and N—H⋯N hydrogen bonds contribute to the planarity of the mol­ecular skeleton. Inter­molecular N—H⋯O hydrogen bonds link the mol­ecules into zigzag chains along the b axis; these mol­ecules are futher paired by π–π inter­actions [cen...

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Detalles Bibliográficos
Autores principales: Zhao, Ren-Gao, Zhang, Wei, Li, Ji-Kun, Zhang, Li-Ya
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2008
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2961450/
https://www.ncbi.nlm.nih.gov/pubmed/21202624
http://dx.doi.org/10.1107/S1600536808014475
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author Zhao, Ren-Gao
Zhang, Wei
Li, Ji-Kun
Zhang, Li-Ya
author_facet Zhao, Ren-Gao
Zhang, Wei
Li, Ji-Kun
Zhang, Li-Ya
author_sort Zhao, Ren-Gao
collection PubMed
description In the title compound, C(9)H(11)N(3)O(2)S, intra­molecular O—H⋯O and N—H⋯N hydrogen bonds contribute to the planarity of the mol­ecular skeleton. Inter­molecular N—H⋯O hydrogen bonds link the mol­ecules into zigzag chains along the b axis; these mol­ecules are futher paired by π–π inter­actions [centroid–centroid distance 4.495 (5) Å]. The crystal structure also exhibits weak inter­molecular N—H⋯S and O—H⋯S hydrogen bonds.
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spelling pubmed-29614502010-12-30 (E)-2-Hydr­oxy-3-methoxy­benzaldehyde thio­semicarbazone Zhao, Ren-Gao Zhang, Wei Li, Ji-Kun Zhang, Li-Ya Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(9)H(11)N(3)O(2)S, intra­molecular O—H⋯O and N—H⋯N hydrogen bonds contribute to the planarity of the mol­ecular skeleton. Inter­molecular N—H⋯O hydrogen bonds link the mol­ecules into zigzag chains along the b axis; these mol­ecules are futher paired by π–π inter­actions [centroid–centroid distance 4.495 (5) Å]. The crystal structure also exhibits weak inter­molecular N—H⋯S and O—H⋯S hydrogen bonds. International Union of Crystallography 2008-05-17 /pmc/articles/PMC2961450/ /pubmed/21202624 http://dx.doi.org/10.1107/S1600536808014475 Text en © Zhao et al. 2008 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Zhao, Ren-Gao
Zhang, Wei
Li, Ji-Kun
Zhang, Li-Ya
(E)-2-Hydr­oxy-3-methoxy­benzaldehyde thio­semicarbazone
title (E)-2-Hydr­oxy-3-methoxy­benzaldehyde thio­semicarbazone
title_full (E)-2-Hydr­oxy-3-methoxy­benzaldehyde thio­semicarbazone
title_fullStr (E)-2-Hydr­oxy-3-methoxy­benzaldehyde thio­semicarbazone
title_full_unstemmed (E)-2-Hydr­oxy-3-methoxy­benzaldehyde thio­semicarbazone
title_short (E)-2-Hydr­oxy-3-methoxy­benzaldehyde thio­semicarbazone
title_sort (e)-2-hydr­oxy-3-methoxy­benzaldehyde thio­semicarbazone
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2961450/
https://www.ncbi.nlm.nih.gov/pubmed/21202624
http://dx.doi.org/10.1107/S1600536808014475
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