3,3′-Bis(4-nitro­phen­yl)-1,1′-(p-phenyl­ene)dithio­urea dimethyl sulfoxide disolvate

The asymmetric unit of the title compound, C(22)H(16)N(6)O(6)S(2)·2C(2)H(6)OS, consists of one half-mol­ecule of the centrosymmetric thiourea derivative and one molecule of dimethyl sulfoxide (DMSO). The carbonyl group forms an intra­molecular hydrogen bond with the NH group, creating a six-membered...

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Autores principales: Dong, Wen-Kui, Yan, Hai-Bo, Chai, Lan-Qin, Lv, Zhong-Wu, Zhao, Chun-Yu
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2008
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2961527/
https://www.ncbi.nlm.nih.gov/pubmed/21202611
http://dx.doi.org/10.1107/S160053680801430X
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author Dong, Wen-Kui
Yan, Hai-Bo
Chai, Lan-Qin
Lv, Zhong-Wu
Zhao, Chun-Yu
author_facet Dong, Wen-Kui
Yan, Hai-Bo
Chai, Lan-Qin
Lv, Zhong-Wu
Zhao, Chun-Yu
author_sort Dong, Wen-Kui
collection PubMed
description The asymmetric unit of the title compound, C(22)H(16)N(6)O(6)S(2)·2C(2)H(6)OS, consists of one half-mol­ecule of the centrosymmetric thiourea derivative and one molecule of dimethyl sulfoxide (DMSO). The carbonyl group forms an intra­molecular hydrogen bond with the NH group, creating a six-membered (C—N—C—N—H⋯O) ring. Two other N—H⋯O hydro­gen bonds link one mol­ecule of the thio­urea to two mol­ecules of DMSO.
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spelling pubmed-29615272010-12-30 3,3′-Bis(4-nitro­phen­yl)-1,1′-(p-phenyl­ene)dithio­urea dimethyl sulfoxide disolvate Dong, Wen-Kui Yan, Hai-Bo Chai, Lan-Qin Lv, Zhong-Wu Zhao, Chun-Yu Acta Crystallogr Sect E Struct Rep Online Organic Papers The asymmetric unit of the title compound, C(22)H(16)N(6)O(6)S(2)·2C(2)H(6)OS, consists of one half-mol­ecule of the centrosymmetric thiourea derivative and one molecule of dimethyl sulfoxide (DMSO). The carbonyl group forms an intra­molecular hydrogen bond with the NH group, creating a six-membered (C—N—C—N—H⋯O) ring. Two other N—H⋯O hydro­gen bonds link one mol­ecule of the thio­urea to two mol­ecules of DMSO. International Union of Crystallography 2008-05-17 /pmc/articles/PMC2961527/ /pubmed/21202611 http://dx.doi.org/10.1107/S160053680801430X Text en © Dong et al. 2008 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Dong, Wen-Kui
Yan, Hai-Bo
Chai, Lan-Qin
Lv, Zhong-Wu
Zhao, Chun-Yu
3,3′-Bis(4-nitro­phen­yl)-1,1′-(p-phenyl­ene)dithio­urea dimethyl sulfoxide disolvate
title 3,3′-Bis(4-nitro­phen­yl)-1,1′-(p-phenyl­ene)dithio­urea dimethyl sulfoxide disolvate
title_full 3,3′-Bis(4-nitro­phen­yl)-1,1′-(p-phenyl­ene)dithio­urea dimethyl sulfoxide disolvate
title_fullStr 3,3′-Bis(4-nitro­phen­yl)-1,1′-(p-phenyl­ene)dithio­urea dimethyl sulfoxide disolvate
title_full_unstemmed 3,3′-Bis(4-nitro­phen­yl)-1,1′-(p-phenyl­ene)dithio­urea dimethyl sulfoxide disolvate
title_short 3,3′-Bis(4-nitro­phen­yl)-1,1′-(p-phenyl­ene)dithio­urea dimethyl sulfoxide disolvate
title_sort 3,3′-bis(4-nitro­phen­yl)-1,1′-(p-phenyl­ene)dithio­urea dimethyl sulfoxide disolvate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2961527/
https://www.ncbi.nlm.nih.gov/pubmed/21202611
http://dx.doi.org/10.1107/S160053680801430X
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