Benzoyl­methyl pyridine-4-carboxyl­ate

In the crystal structure of the title compound, C(14)H(11)NO(3), isolated from the reaction of 2-bromo-1-phenyl­ethanone and pyridine-4-carboxylic acid using triethyl­amine as a base to deprotonate the organic acid, the mol­ecular packing is stabilized by C—H⋯π inter­actions involving the phenyl and...

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Detalles Bibliográficos
Autores principales: Guo, Jian-Nan, Zhang, Bo-Chao, Jin, Yi, Tang, Guo, Zhao, Yu-Fen
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2008
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2961582/
https://www.ncbi.nlm.nih.gov/pubmed/21202617
http://dx.doi.org/10.1107/S1600536808014086
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author Guo, Jian-Nan
Zhang, Bo-Chao
Jin, Yi
Tang, Guo
Zhao, Yu-Fen
author_facet Guo, Jian-Nan
Zhang, Bo-Chao
Jin, Yi
Tang, Guo
Zhao, Yu-Fen
author_sort Guo, Jian-Nan
collection PubMed
description In the crystal structure of the title compound, C(14)H(11)NO(3), isolated from the reaction of 2-bromo-1-phenyl­ethanone and pyridine-4-carboxylic acid using triethyl­amine as a base to deprotonate the organic acid, the mol­ecular packing is stabilized by C—H⋯π inter­actions involving the phenyl and pyridine rings. The C—C—O—C torsion angle for the linkage between the two carbonyl groups is −80.8 (2)°, and the planes of the phenyl and pyridyl rings form a dihedral angle of 65.8 (1)°.
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spelling pubmed-29615822010-12-30 Benzoyl­methyl pyridine-4-carboxyl­ate Guo, Jian-Nan Zhang, Bo-Chao Jin, Yi Tang, Guo Zhao, Yu-Fen Acta Crystallogr Sect E Struct Rep Online Organic Papers In the crystal structure of the title compound, C(14)H(11)NO(3), isolated from the reaction of 2-bromo-1-phenyl­ethanone and pyridine-4-carboxylic acid using triethyl­amine as a base to deprotonate the organic acid, the mol­ecular packing is stabilized by C—H⋯π inter­actions involving the phenyl and pyridine rings. The C—C—O—C torsion angle for the linkage between the two carbonyl groups is −80.8 (2)°, and the planes of the phenyl and pyridyl rings form a dihedral angle of 65.8 (1)°. International Union of Crystallography 2008-05-17 /pmc/articles/PMC2961582/ /pubmed/21202617 http://dx.doi.org/10.1107/S1600536808014086 Text en © Guo et al. 2008 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Guo, Jian-Nan
Zhang, Bo-Chao
Jin, Yi
Tang, Guo
Zhao, Yu-Fen
Benzoyl­methyl pyridine-4-carboxyl­ate
title Benzoyl­methyl pyridine-4-carboxyl­ate
title_full Benzoyl­methyl pyridine-4-carboxyl­ate
title_fullStr Benzoyl­methyl pyridine-4-carboxyl­ate
title_full_unstemmed Benzoyl­methyl pyridine-4-carboxyl­ate
title_short Benzoyl­methyl pyridine-4-carboxyl­ate
title_sort benzoyl­methyl pyridine-4-carboxyl­ate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2961582/
https://www.ncbi.nlm.nih.gov/pubmed/21202617
http://dx.doi.org/10.1107/S1600536808014086
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AT zhangbochao benzoylmethylpyridine4carboxylate
AT jinyi benzoylmethylpyridine4carboxylate
AT tangguo benzoylmethylpyridine4carboxylate
AT zhaoyufen benzoylmethylpyridine4carboxylate

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