5,7,9,10-Tetra­hydro-5β,10β-methano-3aα,8aα-methyl­propenocyclo­octa­[1,2-c:5,6-c′]dipyrazole-3,8(2H,4H)-dione monohydrate

The racemic title compound, C(15)H(16)N(4)O(2)·H(2)O, crystallizes as a hydrogen-bonded layer structure incorporating the solvent water mol­ecules. Within the layers, there are three distinct hydrogen-bonding motifs which can be classified as R (2) (2)(8), R (4) (2)(8) and R (4) (4)(12).

Detalles Bibliográficos
Autores principales: Djaidi, Djamal, Bishop, Roger, Craig, Donald C., Scudder, Marcia L.
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2008
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2961591/
https://www.ncbi.nlm.nih.gov/pubmed/21202574
http://dx.doi.org/10.1107/S1600536808013512
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author Djaidi, Djamal
Bishop, Roger
Craig, Donald C.
Scudder, Marcia L.
author_facet Djaidi, Djamal
Bishop, Roger
Craig, Donald C.
Scudder, Marcia L.
author_sort Djaidi, Djamal
collection PubMed
description The racemic title compound, C(15)H(16)N(4)O(2)·H(2)O, crystallizes as a hydrogen-bonded layer structure incorporating the solvent water mol­ecules. Within the layers, there are three distinct hydrogen-bonding motifs which can be classified as R (2) (2)(8), R (4) (2)(8) and R (4) (4)(12).
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spelling pubmed-29615912010-12-30 5,7,9,10-Tetra­hydro-5β,10β-methano-3aα,8aα-methyl­propenocyclo­octa­[1,2-c:5,6-c′]dipyrazole-3,8(2H,4H)-dione monohydrate Djaidi, Djamal Bishop, Roger Craig, Donald C. Scudder, Marcia L. Acta Crystallogr Sect E Struct Rep Online Organic Papers The racemic title compound, C(15)H(16)N(4)O(2)·H(2)O, crystallizes as a hydrogen-bonded layer structure incorporating the solvent water mol­ecules. Within the layers, there are three distinct hydrogen-bonding motifs which can be classified as R (2) (2)(8), R (4) (2)(8) and R (4) (4)(12). International Union of Crystallography 2008-05-10 /pmc/articles/PMC2961591/ /pubmed/21202574 http://dx.doi.org/10.1107/S1600536808013512 Text en © Djaidi et al. 2008 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Djaidi, Djamal
Bishop, Roger
Craig, Donald C.
Scudder, Marcia L.
5,7,9,10-Tetra­hydro-5β,10β-methano-3aα,8aα-methyl­propenocyclo­octa­[1,2-c:5,6-c′]dipyrazole-3,8(2H,4H)-dione monohydrate
title 5,7,9,10-Tetra­hydro-5β,10β-methano-3aα,8aα-methyl­propenocyclo­octa­[1,2-c:5,6-c′]dipyrazole-3,8(2H,4H)-dione monohydrate
title_full 5,7,9,10-Tetra­hydro-5β,10β-methano-3aα,8aα-methyl­propenocyclo­octa­[1,2-c:5,6-c′]dipyrazole-3,8(2H,4H)-dione monohydrate
title_fullStr 5,7,9,10-Tetra­hydro-5β,10β-methano-3aα,8aα-methyl­propenocyclo­octa­[1,2-c:5,6-c′]dipyrazole-3,8(2H,4H)-dione monohydrate
title_full_unstemmed 5,7,9,10-Tetra­hydro-5β,10β-methano-3aα,8aα-methyl­propenocyclo­octa­[1,2-c:5,6-c′]dipyrazole-3,8(2H,4H)-dione monohydrate
title_short 5,7,9,10-Tetra­hydro-5β,10β-methano-3aα,8aα-methyl­propenocyclo­octa­[1,2-c:5,6-c′]dipyrazole-3,8(2H,4H)-dione monohydrate
title_sort 5,7,9,10-tetra­hydro-5β,10β-methano-3aα,8aα-methyl­propenocyclo­octa­[1,2-c:5,6-c′]dipyrazole-3,8(2h,4h)-dione monohydrate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2961591/
https://www.ncbi.nlm.nih.gov/pubmed/21202574
http://dx.doi.org/10.1107/S1600536808013512
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