N′-(5-Bromo-2-methoxy­benzyl­idene)-3-hydroxy­benzohydrazide methanol hemisolvate

The asymmetric unit of the title compound, C(15)H(13)BrN(2)O(3)·0.5CH(3)OH, contains two Schiff base mol­ecules and a methanol mol­ecule of crystallization. The dihedral angles between the benzene rings in the two mol­ecules are 23.8 (2) and 18.6 (2)°. In the crystal structure, mol­ecules are linked...

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Detalles Bibliográficos
Autor principal: Zhou, Zhi
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2008
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2961683/
https://www.ncbi.nlm.nih.gov/pubmed/21202927
http://dx.doi.org/10.1107/S1600536808018205
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author Zhou, Zhi
author_facet Zhou, Zhi
author_sort Zhou, Zhi
collection PubMed
description The asymmetric unit of the title compound, C(15)H(13)BrN(2)O(3)·0.5CH(3)OH, contains two Schiff base mol­ecules and a methanol mol­ecule of crystallization. The dihedral angles between the benzene rings in the two mol­ecules are 23.8 (2) and 18.6 (2)°. In the crystal structure, mol­ecules are linked through inter­molecular N—H⋯O, O—H⋯O and O—H⋯N hydrogen bonds, forming a three-dimensional network.
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spelling pubmed-29616832010-12-30 N′-(5-Bromo-2-methoxy­benzyl­idene)-3-hydroxy­benzohydrazide methanol hemisolvate Zhou, Zhi Acta Crystallogr Sect E Struct Rep Online Organic Papers The asymmetric unit of the title compound, C(15)H(13)BrN(2)O(3)·0.5CH(3)OH, contains two Schiff base mol­ecules and a methanol mol­ecule of crystallization. The dihedral angles between the benzene rings in the two mol­ecules are 23.8 (2) and 18.6 (2)°. In the crystal structure, mol­ecules are linked through inter­molecular N—H⋯O, O—H⋯O and O—H⋯N hydrogen bonds, forming a three-dimensional network. International Union of Crystallography 2008-06-19 /pmc/articles/PMC2961683/ /pubmed/21202927 http://dx.doi.org/10.1107/S1600536808018205 Text en © Zhi Zhou 2008 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Zhou, Zhi
N′-(5-Bromo-2-methoxy­benzyl­idene)-3-hydroxy­benzohydrazide methanol hemisolvate
title N′-(5-Bromo-2-methoxy­benzyl­idene)-3-hydroxy­benzohydrazide methanol hemisolvate
title_full N′-(5-Bromo-2-methoxy­benzyl­idene)-3-hydroxy­benzohydrazide methanol hemisolvate
title_fullStr N′-(5-Bromo-2-methoxy­benzyl­idene)-3-hydroxy­benzohydrazide methanol hemisolvate
title_full_unstemmed N′-(5-Bromo-2-methoxy­benzyl­idene)-3-hydroxy­benzohydrazide methanol hemisolvate
title_short N′-(5-Bromo-2-methoxy­benzyl­idene)-3-hydroxy­benzohydrazide methanol hemisolvate
title_sort n′-(5-bromo-2-methoxy­benzyl­idene)-3-hydroxy­benzohydrazide methanol hemisolvate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2961683/
https://www.ncbi.nlm.nih.gov/pubmed/21202927
http://dx.doi.org/10.1107/S1600536808018205
work_keys_str_mv AT zhouzhi n5bromo2methoxybenzylidene3hydroxybenzohydrazidemethanolhemisolvate

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