Cytenamide–butyric acid (1/1)

Cytenamide forms a 1:1 solvate with butyric acid [systematic name: 5H-dibenzo[a,d]cyclo­hepta­triene-5-carboxamide–butanoic acid (1/1)], C(16)H(13)NO·C(4)H(8)O(2). The title compound crystallizes with one mol­ecule of cytenamide and one of butyric acid in the asymmetric unit; these mol­ecules are li...

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Detalles Bibliográficos
Autores principales: Johnston, Andrea, Florence, Alastair J., Fabbiani, Francesca J. A., Shankland, Kenneth, Bedford, Colin T.
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2008
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2961685/
https://www.ncbi.nlm.nih.gov/pubmed/21202925
http://dx.doi.org/10.1107/S1600536808018059
Descripción
Sumario:Cytenamide forms a 1:1 solvate with butyric acid [systematic name: 5H-dibenzo[a,d]cyclo­hepta­triene-5-carboxamide–butanoic acid (1/1)], C(16)H(13)NO·C(4)H(8)O(2). The title compound crystallizes with one mol­ecule of cytenamide and one of butyric acid in the asymmetric unit; these mol­ecules are linked by N—H⋯O and O—H⋯O hydrogen bonds to form an R (2) (2)(8) heterodimer motif. Pairs of adjacent motifs are further connected via N—H⋯O inter­actions to form a discrete centrosymmetric assembly.

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