3,5-Bis[1-acetyl-5-(4-chloro­phen­yl)-4,5-dihydro-1H-pyrazol-3-yl]-2,6-dimethyl­pyridine tetra­hydro­furan solvate

In the title compound, C(29)H(27)Cl(2)N(5)O(2)·C(4)H(8)O, the polycyclic system is composed of three parts: one central pyridine ring substituted by two functionalized pyrazoline rings. The dihedral angles between the central pyridine plane and pyrazoline planes are 5.11 (1) and 13.99 (1)°, whereas...

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Detalles Bibliográficos
Autores principales: Qian, Qun, Zhang, Jun, Zhang, Min, He, Xiang, Xia, YiBen
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2008
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2961714/
https://www.ncbi.nlm.nih.gov/pubmed/21202958
http://dx.doi.org/10.1107/S1600536808018497
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author Qian, Qun
Zhang, Jun
Zhang, Min
He, Xiang
Xia, YiBen
author_facet Qian, Qun
Zhang, Jun
Zhang, Min
He, Xiang
Xia, YiBen
author_sort Qian, Qun
collection PubMed
description In the title compound, C(29)H(27)Cl(2)N(5)O(2)·C(4)H(8)O, the polycyclic system is composed of three parts: one central pyridine ring substituted by two functionalized pyrazoline rings. The dihedral angles between the central pyridine plane and pyrazoline planes are 5.11 (1) and 13.99 (1)°, whereas the dihedral angles between each chloro­phenyl plane and the attached pyrazoline planes are 88.65 (1) and 83.87 (1)°. Mol­ecules are linked by inter­molecular C—H⋯O hydrogen bonds, forming a three-dimensional network.
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spelling pubmed-29617142010-12-30 3,5-Bis[1-acetyl-5-(4-chloro­phen­yl)-4,5-dihydro-1H-pyrazol-3-yl]-2,6-dimethyl­pyridine tetra­hydro­furan solvate Qian, Qun Zhang, Jun Zhang, Min He, Xiang Xia, YiBen Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(29)H(27)Cl(2)N(5)O(2)·C(4)H(8)O, the polycyclic system is composed of three parts: one central pyridine ring substituted by two functionalized pyrazoline rings. The dihedral angles between the central pyridine plane and pyrazoline planes are 5.11 (1) and 13.99 (1)°, whereas the dihedral angles between each chloro­phenyl plane and the attached pyrazoline planes are 88.65 (1) and 83.87 (1)°. Mol­ecules are linked by inter­molecular C—H⋯O hydrogen bonds, forming a three-dimensional network. International Union of Crystallography 2008-06-25 /pmc/articles/PMC2961714/ /pubmed/21202958 http://dx.doi.org/10.1107/S1600536808018497 Text en © Qian et al. 2008 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Qian, Qun
Zhang, Jun
Zhang, Min
He, Xiang
Xia, YiBen
3,5-Bis[1-acetyl-5-(4-chloro­phen­yl)-4,5-dihydro-1H-pyrazol-3-yl]-2,6-dimethyl­pyridine tetra­hydro­furan solvate
title 3,5-Bis[1-acetyl-5-(4-chloro­phen­yl)-4,5-dihydro-1H-pyrazol-3-yl]-2,6-dimethyl­pyridine tetra­hydro­furan solvate
title_full 3,5-Bis[1-acetyl-5-(4-chloro­phen­yl)-4,5-dihydro-1H-pyrazol-3-yl]-2,6-dimethyl­pyridine tetra­hydro­furan solvate
title_fullStr 3,5-Bis[1-acetyl-5-(4-chloro­phen­yl)-4,5-dihydro-1H-pyrazol-3-yl]-2,6-dimethyl­pyridine tetra­hydro­furan solvate
title_full_unstemmed 3,5-Bis[1-acetyl-5-(4-chloro­phen­yl)-4,5-dihydro-1H-pyrazol-3-yl]-2,6-dimethyl­pyridine tetra­hydro­furan solvate
title_short 3,5-Bis[1-acetyl-5-(4-chloro­phen­yl)-4,5-dihydro-1H-pyrazol-3-yl]-2,6-dimethyl­pyridine tetra­hydro­furan solvate
title_sort 3,5-bis[1-acetyl-5-(4-chloro­phen­yl)-4,5-dihydro-1h-pyrazol-3-yl]-2,6-dimethyl­pyridine tetra­hydro­furan solvate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2961714/
https://www.ncbi.nlm.nih.gov/pubmed/21202958
http://dx.doi.org/10.1107/S1600536808018497
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