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(E)-1-(3-Methoxy­phen­yl)ethanone 4-nitro­phenyl­hydrazone

Crystals of the title compound, C(15)H(15)N(3)O(3), were obtained from a condensation reaction of 4-nitro­phenyl­hydrazine and 3-methoxy­acetophenone. In the crystal structure, the methoxy­phenyl ring is twisted slightly with respect to the nitro­phenyl­hydrazine plane, making a dihedral angle of 14...

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Detalles Bibliográficos
Autores principales: Fan, Zheng, Shan, Shang, Wang, Shan-Heng, Wang, Wen-Long
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2008
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2961743/
https://www.ncbi.nlm.nih.gov/pubmed/21202963
http://dx.doi.org/10.1107/S1600536808018618
Descripción
Sumario:Crystals of the title compound, C(15)H(15)N(3)O(3), were obtained from a condensation reaction of 4-nitro­phenyl­hydrazine and 3-methoxy­acetophenone. In the crystal structure, the methoxy­phenyl ring is twisted slightly with respect to the nitro­phenyl­hydrazine plane, making a dihedral angle of 14.81 (8)°. The nitro and meth­oxy groups are each coplanar with the attached benzene rings. The nitro­phenyl and methoxy­phenyl groups are located on opposite sides of the C=N double bond, indicating an E configuration of the mol­ecule. Adjacent mol­ecules are linked together via N—H⋯O hydrogen bonding, forming chains along the [101] direction.