Ethyl 2-{N-[N-(4-chloro-6-methoxy­pyrimidin-2-yl)carbamo­yl]sulfamo­yl}benzoate

The asymmetric unit of the title compound, C(15)H(15)ClN(4)O(6)S, contains two independent mol­ecules, in which the pyrimidine and benzene rings are oriented at dihedral angles of 75.21 (3) and 86.00 (3)°. Intra­molecular N—H⋯N and C—H⋯O hydrogen bonds result in the formation of two five- and two si...

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Detalles Bibliográficos
Autores principales: Lu, Chui, Li, Fang-Shi, Yu, Da-Sheng, Yao, Wei, Liu, Yin-Hong
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2008
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2961814/
https://www.ncbi.nlm.nih.gov/pubmed/21202882
http://dx.doi.org/10.1107/S1600536808017029
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author Lu, Chui
Li, Fang-Shi
Yu, Da-Sheng
Yao, Wei
Liu, Yin-Hong
author_facet Lu, Chui
Li, Fang-Shi
Yu, Da-Sheng
Yao, Wei
Liu, Yin-Hong
author_sort Lu, Chui
collection PubMed
description The asymmetric unit of the title compound, C(15)H(15)ClN(4)O(6)S, contains two independent mol­ecules, in which the pyrimidine and benzene rings are oriented at dihedral angles of 75.21 (3) and 86.00 (3)°. Intra­molecular N—H⋯N and C—H⋯O hydrogen bonds result in the formation of two five- and two six-membered rings. The six-membered rings have flattened-boat conformations, while the five-membered rings adopt envelope conformations. In the crystal structure, inter­molecular N—H⋯O hydrogen bonds link the mol­ecules.
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spelling pubmed-29618142010-12-30 Ethyl 2-{N-[N-(4-chloro-6-methoxy­pyrimidin-2-yl)carbamo­yl]sulfamo­yl}benzoate Lu, Chui Li, Fang-Shi Yu, Da-Sheng Yao, Wei Liu, Yin-Hong Acta Crystallogr Sect E Struct Rep Online Organic Papers The asymmetric unit of the title compound, C(15)H(15)ClN(4)O(6)S, contains two independent mol­ecules, in which the pyrimidine and benzene rings are oriented at dihedral angles of 75.21 (3) and 86.00 (3)°. Intra­molecular N—H⋯N and C—H⋯O hydrogen bonds result in the formation of two five- and two six-membered rings. The six-membered rings have flattened-boat conformations, while the five-membered rings adopt envelope conformations. In the crystal structure, inter­molecular N—H⋯O hydrogen bonds link the mol­ecules. International Union of Crystallography 2008-06-13 /pmc/articles/PMC2961814/ /pubmed/21202882 http://dx.doi.org/10.1107/S1600536808017029 Text en © Lu et al. 2008 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Lu, Chui
Li, Fang-Shi
Yu, Da-Sheng
Yao, Wei
Liu, Yin-Hong
Ethyl 2-{N-[N-(4-chloro-6-methoxy­pyrimidin-2-yl)carbamo­yl]sulfamo­yl}benzoate
title Ethyl 2-{N-[N-(4-chloro-6-methoxy­pyrimidin-2-yl)carbamo­yl]sulfamo­yl}benzoate
title_full Ethyl 2-{N-[N-(4-chloro-6-methoxy­pyrimidin-2-yl)carbamo­yl]sulfamo­yl}benzoate
title_fullStr Ethyl 2-{N-[N-(4-chloro-6-methoxy­pyrimidin-2-yl)carbamo­yl]sulfamo­yl}benzoate
title_full_unstemmed Ethyl 2-{N-[N-(4-chloro-6-methoxy­pyrimidin-2-yl)carbamo­yl]sulfamo­yl}benzoate
title_short Ethyl 2-{N-[N-(4-chloro-6-methoxy­pyrimidin-2-yl)carbamo­yl]sulfamo­yl}benzoate
title_sort ethyl 2-{n-[n-(4-chloro-6-methoxy­pyrimidin-2-yl)carbamo­yl]sulfamo­yl}benzoate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2961814/
https://www.ncbi.nlm.nih.gov/pubmed/21202882
http://dx.doi.org/10.1107/S1600536808017029
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