2,2′-(3,5-Dinitro­benzyl­imino)diethanol

The title compound, C(11)H(15)N(3)O(6), was prepared by the reaction of (3,5-dinitro­benz­yl)methane­sulfonate with diethanol­amine. The asymmetric unit contains four crystallographically independent mol­ecules which differ primarily in their rotation about the bond between the aromatic ring and the...

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Detalles Bibliográficos
Autores principales: Khan, Gul S., Clark, George R., Barker, David
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2008
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2961823/
https://www.ncbi.nlm.nih.gov/pubmed/21202887
http://dx.doi.org/10.1107/S1600536808017066
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author Khan, Gul S.
Clark, George R.
Barker, David
author_facet Khan, Gul S.
Clark, George R.
Barker, David
author_sort Khan, Gul S.
collection PubMed
description The title compound, C(11)H(15)N(3)O(6), was prepared by the reaction of (3,5-dinitro­benz­yl)methane­sulfonate with diethanol­amine. The asymmetric unit contains four crystallographically independent mol­ecules which differ primarily in their rotation about the bond between the aromatic ring and the N-diethanol unit. The mol­ecules are linked into sheets by a hydrogen-bonding network which involves all of the hydroxy groups, with only van der Waals contacts between the sheets.
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spelling pubmed-29618232010-12-30 2,2′-(3,5-Dinitro­benzyl­imino)diethanol Khan, Gul S. Clark, George R. Barker, David Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(11)H(15)N(3)O(6), was prepared by the reaction of (3,5-dinitro­benz­yl)methane­sulfonate with diethanol­amine. The asymmetric unit contains four crystallographically independent mol­ecules which differ primarily in their rotation about the bond between the aromatic ring and the N-diethanol unit. The mol­ecules are linked into sheets by a hydrogen-bonding network which involves all of the hydroxy groups, with only van der Waals contacts between the sheets. International Union of Crystallography 2008-06-13 /pmc/articles/PMC2961823/ /pubmed/21202887 http://dx.doi.org/10.1107/S1600536808017066 Text en © Khan et al. 2008 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Khan, Gul S.
Clark, George R.
Barker, David
2,2′-(3,5-Dinitro­benzyl­imino)diethanol
title 2,2′-(3,5-Dinitro­benzyl­imino)diethanol
title_full 2,2′-(3,5-Dinitro­benzyl­imino)diethanol
title_fullStr 2,2′-(3,5-Dinitro­benzyl­imino)diethanol
title_full_unstemmed 2,2′-(3,5-Dinitro­benzyl­imino)diethanol
title_short 2,2′-(3,5-Dinitro­benzyl­imino)diethanol
title_sort 2,2′-(3,5-dinitro­benzyl­imino)diethanol
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2961823/
https://www.ncbi.nlm.nih.gov/pubmed/21202887
http://dx.doi.org/10.1107/S1600536808017066
work_keys_str_mv AT khanguls 2235dinitrobenzyliminodiethanol
AT clarkgeorger 2235dinitrobenzyliminodiethanol
AT barkerdavid 2235dinitrobenzyliminodiethanol

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