Benzene-1,3,5-tricarboxylic acid–1,2-bis­(1,2,4-triazol-4-yl)ethane–water (4/1/2)

The title compound, 4C(9)H(6)O(6)·C(6)H(8)N(6)·2H(2)O, crystallizes in a layer structure where each sheet is composed of anellated hydrogen-bonded rings of six distinct sizes: R (2) (2)(16), R (3) (3)(18), R (4) (4)(12), R (4) (4)(18), R (4) (4)(22) and R (4) (4)(25). The two largest rings, viz. R (...

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Detalles Bibliográficos
Autores principales: Habib, Hesham A., Janiak, Christoph
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2008
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2961855/
https://www.ncbi.nlm.nih.gov/pubmed/21202840
http://dx.doi.org/10.1107/S1600536808015808
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author Habib, Hesham A.
Janiak, Christoph
author_facet Habib, Hesham A.
Janiak, Christoph
author_sort Habib, Hesham A.
collection PubMed
description The title compound, 4C(9)H(6)O(6)·C(6)H(8)N(6)·2H(2)O, crystallizes in a layer structure where each sheet is composed of anellated hydrogen-bonded rings of six distinct sizes: R (2) (2)(16), R (3) (3)(18), R (4) (4)(12), R (4) (4)(18), R (4) (4)(22) and R (4) (4)(25). The two largest rings, viz. R (4) (4)(22) and R (4) (4)(25), are associated with O—H⋯N bonds from the carboxyl groups to the triazole rings. The typical head-to-tail carbox­yl–carboxyl R (2) (2)(8) motif is not observed.
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spelling pubmed-29618552010-12-30 Benzene-1,3,5-tricarboxylic acid–1,2-bis­(1,2,4-triazol-4-yl)ethane–water (4/1/2) Habib, Hesham A. Janiak, Christoph Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, 4C(9)H(6)O(6)·C(6)H(8)N(6)·2H(2)O, crystallizes in a layer structure where each sheet is composed of anellated hydrogen-bonded rings of six distinct sizes: R (2) (2)(16), R (3) (3)(18), R (4) (4)(12), R (4) (4)(18), R (4) (4)(22) and R (4) (4)(25). The two largest rings, viz. R (4) (4)(22) and R (4) (4)(25), are associated with O—H⋯N bonds from the carboxyl groups to the triazole rings. The typical head-to-tail carbox­yl–carboxyl R (2) (2)(8) motif is not observed. International Union of Crystallography 2008-06-07 /pmc/articles/PMC2961855/ /pubmed/21202840 http://dx.doi.org/10.1107/S1600536808015808 Text en © Habib and Janiak 2008 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Habib, Hesham A.
Janiak, Christoph
Benzene-1,3,5-tricarboxylic acid–1,2-bis­(1,2,4-triazol-4-yl)ethane–water (4/1/2)
title Benzene-1,3,5-tricarboxylic acid–1,2-bis­(1,2,4-triazol-4-yl)ethane–water (4/1/2)
title_full Benzene-1,3,5-tricarboxylic acid–1,2-bis­(1,2,4-triazol-4-yl)ethane–water (4/1/2)
title_fullStr Benzene-1,3,5-tricarboxylic acid–1,2-bis­(1,2,4-triazol-4-yl)ethane–water (4/1/2)
title_full_unstemmed Benzene-1,3,5-tricarboxylic acid–1,2-bis­(1,2,4-triazol-4-yl)ethane–water (4/1/2)
title_short Benzene-1,3,5-tricarboxylic acid–1,2-bis­(1,2,4-triazol-4-yl)ethane–water (4/1/2)
title_sort benzene-1,3,5-tricarboxylic acid–1,2-bis­(1,2,4-triazol-4-yl)ethane–water (4/1/2)
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2961855/
https://www.ncbi.nlm.nih.gov/pubmed/21202840
http://dx.doi.org/10.1107/S1600536808015808
work_keys_str_mv AT habibheshama benzene135tricarboxylicacid12bis124triazol4ylethanewater412
AT janiakchristoph benzene135tricarboxylicacid12bis124triazol4ylethanewater412

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