N′-(2-Chloro-5-nitro­benzyl­idene)-3-hydroxy­benzohydrazide methanol solvate

In the title compound, C(14)H(10)ClN(3)O(4)·CH(3)OH, the dihedral angle between the two benzene rings is 33.9 (2)°. In the crystal structure, the methanol solvent mol­ecules are linked to the Schiff base mol­ecules through inter­molecular N—H⋯O and O—H⋯O hydrogen bonds. Mol­ecules are further linked...

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Detalles Bibliográficos
Autor principal: Zhou, Zhi
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2008
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2962016/
https://www.ncbi.nlm.nih.gov/pubmed/21203103
http://dx.doi.org/10.1107/S1600536808019636
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author Zhou, Zhi
author_facet Zhou, Zhi
author_sort Zhou, Zhi
collection PubMed
description In the title compound, C(14)H(10)ClN(3)O(4)·CH(3)OH, the dihedral angle between the two benzene rings is 33.9 (2)°. In the crystal structure, the methanol solvent mol­ecules are linked to the Schiff base mol­ecules through inter­molecular N—H⋯O and O—H⋯O hydrogen bonds. Mol­ecules are further linked through inter­molecular O—H⋯O and O—H⋯N hydrogen bonds, forming chains running along the b axis.
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spelling pubmed-29620162010-12-30 N′-(2-Chloro-5-nitro­benzyl­idene)-3-hydroxy­benzohydrazide methanol solvate Zhou, Zhi Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(14)H(10)ClN(3)O(4)·CH(3)OH, the dihedral angle between the two benzene rings is 33.9 (2)°. In the crystal structure, the methanol solvent mol­ecules are linked to the Schiff base mol­ecules through inter­molecular N—H⋯O and O—H⋯O hydrogen bonds. Mol­ecules are further linked through inter­molecular O—H⋯O and O—H⋯N hydrogen bonds, forming chains running along the b axis. International Union of Crystallography 2008-07-05 /pmc/articles/PMC2962016/ /pubmed/21203103 http://dx.doi.org/10.1107/S1600536808019636 Text en © Zhi Zhou 2008 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Zhou, Zhi
N′-(2-Chloro-5-nitro­benzyl­idene)-3-hydroxy­benzohydrazide methanol solvate
title N′-(2-Chloro-5-nitro­benzyl­idene)-3-hydroxy­benzohydrazide methanol solvate
title_full N′-(2-Chloro-5-nitro­benzyl­idene)-3-hydroxy­benzohydrazide methanol solvate
title_fullStr N′-(2-Chloro-5-nitro­benzyl­idene)-3-hydroxy­benzohydrazide methanol solvate
title_full_unstemmed N′-(2-Chloro-5-nitro­benzyl­idene)-3-hydroxy­benzohydrazide methanol solvate
title_short N′-(2-Chloro-5-nitro­benzyl­idene)-3-hydroxy­benzohydrazide methanol solvate
title_sort n′-(2-chloro-5-nitro­benzyl­idene)-3-hydroxy­benzohydrazide methanol solvate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2962016/
https://www.ncbi.nlm.nih.gov/pubmed/21203103
http://dx.doi.org/10.1107/S1600536808019636
work_keys_str_mv AT zhouzhi n2chloro5nitrobenzylidene3hydroxybenzohydrazidemethanolsolvate

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