1-[2-(3,4-Dichloro­phen­yl)-5-(3,4,5-trimethoxy­phen­yl)-2,3-dihydro-1,3,4-oxadiazol-3-yl]ethanone

The title compound, C(19)H(18)Cl(2)N(2)O(5), was synthesized by the reaction of N′-(3,4-dichloro­benzyl­idene)-3,4,5-trimethoxy­benzo­hydrazide and acetic anhydride. The oxadiazole ring makes dihedral angles of 82.82 (7) and 9.92 (7)° with the 3,4-dichloro­benzene and the 3,4,5-trimethoxy­benzene ri...

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Detalles Bibliográficos
Autores principales: He, Dao-Hang, Zhu, Yong-Chuang
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2008
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2962074/
https://www.ncbi.nlm.nih.gov/pubmed/21203158
http://dx.doi.org/10.1107/S1600536808020771
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author He, Dao-Hang
Zhu, Yong-Chuang
author_facet He, Dao-Hang
Zhu, Yong-Chuang
author_sort He, Dao-Hang
collection PubMed
description The title compound, C(19)H(18)Cl(2)N(2)O(5), was synthesized by the reaction of N′-(3,4-dichloro­benzyl­idene)-3,4,5-trimethoxy­benzo­hydrazide and acetic anhydride. The oxadiazole ring makes dihedral angles of 82.82 (7) and 9.92 (7)° with the 3,4-dichloro­benzene and the 3,4,5-trimethoxy­benzene ring planes, respectively. The crystal structure is stabilized by inter­molecular C—H⋯ O and C—H⋯ N hydrogen bonds. Intra­molecular C—H⋯O and C—H⋯N hydrogen bonds are also present.
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spelling pubmed-29620742010-12-30 1-[2-(3,4-Dichloro­phen­yl)-5-(3,4,5-trimethoxy­phen­yl)-2,3-dihydro-1,3,4-oxadiazol-3-yl]ethanone He, Dao-Hang Zhu, Yong-Chuang Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(19)H(18)Cl(2)N(2)O(5), was synthesized by the reaction of N′-(3,4-dichloro­benzyl­idene)-3,4,5-trimethoxy­benzo­hydrazide and acetic anhydride. The oxadiazole ring makes dihedral angles of 82.82 (7) and 9.92 (7)° with the 3,4-dichloro­benzene and the 3,4,5-trimethoxy­benzene ring planes, respectively. The crystal structure is stabilized by inter­molecular C—H⋯ O and C—H⋯ N hydrogen bonds. Intra­molecular C—H⋯O and C—H⋯N hydrogen bonds are also present. International Union of Crystallography 2008-07-09 /pmc/articles/PMC2962074/ /pubmed/21203158 http://dx.doi.org/10.1107/S1600536808020771 Text en © He and Zhu 2008 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
He, Dao-Hang
Zhu, Yong-Chuang
1-[2-(3,4-Dichloro­phen­yl)-5-(3,4,5-trimethoxy­phen­yl)-2,3-dihydro-1,3,4-oxadiazol-3-yl]ethanone
title 1-[2-(3,4-Dichloro­phen­yl)-5-(3,4,5-trimethoxy­phen­yl)-2,3-dihydro-1,3,4-oxadiazol-3-yl]ethanone
title_full 1-[2-(3,4-Dichloro­phen­yl)-5-(3,4,5-trimethoxy­phen­yl)-2,3-dihydro-1,3,4-oxadiazol-3-yl]ethanone
title_fullStr 1-[2-(3,4-Dichloro­phen­yl)-5-(3,4,5-trimethoxy­phen­yl)-2,3-dihydro-1,3,4-oxadiazol-3-yl]ethanone
title_full_unstemmed 1-[2-(3,4-Dichloro­phen­yl)-5-(3,4,5-trimethoxy­phen­yl)-2,3-dihydro-1,3,4-oxadiazol-3-yl]ethanone
title_short 1-[2-(3,4-Dichloro­phen­yl)-5-(3,4,5-trimethoxy­phen­yl)-2,3-dihydro-1,3,4-oxadiazol-3-yl]ethanone
title_sort 1-[2-(3,4-dichloro­phen­yl)-5-(3,4,5-trimethoxy­phen­yl)-2,3-dihydro-1,3,4-oxadiazol-3-yl]ethanone
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2962074/
https://www.ncbi.nlm.nih.gov/pubmed/21203158
http://dx.doi.org/10.1107/S1600536808020771
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AT zhuyongchuang 1234dichlorophenyl5345trimethoxyphenyl23dihydro134oxadiazol3ylethanone

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