N-(2-Furylcarbon­yl)piperidine-1-carbo­thio­amide

The title compound, C(11)H(14)N(2)O(2)S, was synthesized from furoyl isothio­cyanate and piperidine in dry acetone. The thio­urea group is in the thio­amide form. The thio­urea group makes a dihedral angle of 53.9 (1)° with the furan carbonyl group. In the crystal structure, mol­ecules are linked by...

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Detalles Bibliográficos
Autores principales: Duque, J., Estévez-Hernández, O., Mascarenhas, Yvonne, Ellena, J., Corrêa, Rodrigo S.
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2008
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2962087/
https://www.ncbi.nlm.nih.gov/pubmed/21203171
http://dx.doi.org/10.1107/S1600536808020977
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author Duque, J.
Estévez-Hernández, O.
Mascarenhas, Yvonne
Ellena, J.
Corrêa, Rodrigo S.
author_facet Duque, J.
Estévez-Hernández, O.
Mascarenhas, Yvonne
Ellena, J.
Corrêa, Rodrigo S.
author_sort Duque, J.
collection PubMed
description The title compound, C(11)H(14)N(2)O(2)S, was synthesized from furoyl isothio­cyanate and piperidine in dry acetone. The thio­urea group is in the thio­amide form. The thio­urea group makes a dihedral angle of 53.9 (1)° with the furan carbonyl group. In the crystal structure, mol­ecules are linked by inter­molecular N—H⋯O hydrogen bonds, forming one-dimensional chains along the c axis. An intramolecular N—H⋯O hydrogen bond is also present.
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spelling pubmed-29620872010-12-30 N-(2-Furylcarbon­yl)piperidine-1-carbo­thio­amide Duque, J. Estévez-Hernández, O. Mascarenhas, Yvonne Ellena, J. Corrêa, Rodrigo S. Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(11)H(14)N(2)O(2)S, was synthesized from furoyl isothio­cyanate and piperidine in dry acetone. The thio­urea group is in the thio­amide form. The thio­urea group makes a dihedral angle of 53.9 (1)° with the furan carbonyl group. In the crystal structure, mol­ecules are linked by inter­molecular N—H⋯O hydrogen bonds, forming one-dimensional chains along the c axis. An intramolecular N—H⋯O hydrogen bond is also present. International Union of Crystallography 2008-07-12 /pmc/articles/PMC2962087/ /pubmed/21203171 http://dx.doi.org/10.1107/S1600536808020977 Text en © Duque et al. 2008 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Duque, J.
Estévez-Hernández, O.
Mascarenhas, Yvonne
Ellena, J.
Corrêa, Rodrigo S.
N-(2-Furylcarbon­yl)piperidine-1-carbo­thio­amide
title N-(2-Furylcarbon­yl)piperidine-1-carbo­thio­amide
title_full N-(2-Furylcarbon­yl)piperidine-1-carbo­thio­amide
title_fullStr N-(2-Furylcarbon­yl)piperidine-1-carbo­thio­amide
title_full_unstemmed N-(2-Furylcarbon­yl)piperidine-1-carbo­thio­amide
title_short N-(2-Furylcarbon­yl)piperidine-1-carbo­thio­amide
title_sort n-(2-furylcarbon­yl)piperidine-1-carbo­thio­amide
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2962087/
https://www.ncbi.nlm.nih.gov/pubmed/21203171
http://dx.doi.org/10.1107/S1600536808020977
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AT mascarenhasyvonne n2furylcarbonylpiperidine1carbothioamide
AT ellenaj n2furylcarbonylpiperidine1carbothioamide
AT correarodrigos n2furylcarbonylpiperidine1carbothioamide

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