1,1′,5,5′-Tetra­methyl-2,2′-diphenyl-4,4′-[p-phenyl­enebis(methyl­idynenitrilo)]di-1H-pyrazol-3(2H)-one

In the centrosymmetric title compound, C(30)H(28)N(6)O(2), the dihedral angles between the anti­pyrine ring and the terminal phenyl and central benzene rings are 50.55 (10) and 14.62 (9)°, respectively. Some short inter­molecular C—H⋯O inter­actions may help to establish the packing. An intramolecul...

Descripción completa

Detalles Bibliográficos
Autores principales: Xiao, Yan, Bi, Cai Feng, Wang, Ai Dong, Fan, Yu Hua, Zhang, Xia, Xu, Jia Kun, Xie, Si Tang
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2008
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2962109/
https://www.ncbi.nlm.nih.gov/pubmed/21203191
http://dx.doi.org/10.1107/S1600536808021028
_version_ 1782189142396895232
author Xiao, Yan
Bi, Cai Feng
Wang, Ai Dong
Fan, Yu Hua
Zhang, Xia
Xu, Jia Kun
Xie, Si Tang
author_facet Xiao, Yan
Bi, Cai Feng
Wang, Ai Dong
Fan, Yu Hua
Zhang, Xia
Xu, Jia Kun
Xie, Si Tang
author_sort Xiao, Yan
collection PubMed
description In the centrosymmetric title compound, C(30)H(28)N(6)O(2), the dihedral angles between the anti­pyrine ring and the terminal phenyl and central benzene rings are 50.55 (10) and 14.62 (9)°, respectively. Some short inter­molecular C—H⋯O inter­actions may help to establish the packing. An intramolecular C—H⋯O hydrogen bond is also present.
format Text
id pubmed-2962109
institution National Center for Biotechnology Information
language English
publishDate 2008
publisher International Union of Crystallography
record_format MEDLINE/PubMed
spelling pubmed-29621092010-12-30 1,1′,5,5′-Tetra­methyl-2,2′-diphenyl-4,4′-[p-phenyl­enebis(methyl­idynenitrilo)]di-1H-pyrazol-3(2H)-one Xiao, Yan Bi, Cai Feng Wang, Ai Dong Fan, Yu Hua Zhang, Xia Xu, Jia Kun Xie, Si Tang Acta Crystallogr Sect E Struct Rep Online Organic Papers In the centrosymmetric title compound, C(30)H(28)N(6)O(2), the dihedral angles between the anti­pyrine ring and the terminal phenyl and central benzene rings are 50.55 (10) and 14.62 (9)°, respectively. Some short inter­molecular C—H⋯O inter­actions may help to establish the packing. An intramolecular C—H⋯O hydrogen bond is also present. International Union of Crystallography 2008-07-12 /pmc/articles/PMC2962109/ /pubmed/21203191 http://dx.doi.org/10.1107/S1600536808021028 Text en © Xiao et al. 2008 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Xiao, Yan
Bi, Cai Feng
Wang, Ai Dong
Fan, Yu Hua
Zhang, Xia
Xu, Jia Kun
Xie, Si Tang
1,1′,5,5′-Tetra­methyl-2,2′-diphenyl-4,4′-[p-phenyl­enebis(methyl­idynenitrilo)]di-1H-pyrazol-3(2H)-one
title 1,1′,5,5′-Tetra­methyl-2,2′-diphenyl-4,4′-[p-phenyl­enebis(methyl­idynenitrilo)]di-1H-pyrazol-3(2H)-one
title_full 1,1′,5,5′-Tetra­methyl-2,2′-diphenyl-4,4′-[p-phenyl­enebis(methyl­idynenitrilo)]di-1H-pyrazol-3(2H)-one
title_fullStr 1,1′,5,5′-Tetra­methyl-2,2′-diphenyl-4,4′-[p-phenyl­enebis(methyl­idynenitrilo)]di-1H-pyrazol-3(2H)-one
title_full_unstemmed 1,1′,5,5′-Tetra­methyl-2,2′-diphenyl-4,4′-[p-phenyl­enebis(methyl­idynenitrilo)]di-1H-pyrazol-3(2H)-one
title_short 1,1′,5,5′-Tetra­methyl-2,2′-diphenyl-4,4′-[p-phenyl­enebis(methyl­idynenitrilo)]di-1H-pyrazol-3(2H)-one
title_sort 1,1′,5,5′-tetra­methyl-2,2′-diphenyl-4,4′-[p-phenyl­enebis(methyl­idynenitrilo)]di-1h-pyrazol-3(2h)-one
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2962109/
https://www.ncbi.nlm.nih.gov/pubmed/21203191
http://dx.doi.org/10.1107/S1600536808021028
work_keys_str_mv AT xiaoyan 1155tetramethyl22diphenyl44pphenylenebismethylidynenitrilodi1hpyrazol32hone
AT bicaifeng 1155tetramethyl22diphenyl44pphenylenebismethylidynenitrilodi1hpyrazol32hone
AT wangaidong 1155tetramethyl22diphenyl44pphenylenebismethylidynenitrilodi1hpyrazol32hone
AT fanyuhua 1155tetramethyl22diphenyl44pphenylenebismethylidynenitrilodi1hpyrazol32hone
AT zhangxia 1155tetramethyl22diphenyl44pphenylenebismethylidynenitrilodi1hpyrazol32hone
AT xujiakun 1155tetramethyl22diphenyl44pphenylenebismethylidynenitrilodi1hpyrazol32hone
AT xiesitang 1155tetramethyl22diphenyl44pphenylenebismethylidynenitrilodi1hpyrazol32hone

Ejemplares similares